N-OCTYLBENZENE synthesis
- Product Name:N-OCTYLBENZENE
- CAS Number:2189-60-8
- Molecular formula:C14H22
- Molecular Weight:190.32
111-83-1
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98-80-6
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2189-60-8
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$30.00/20mg
Yield:2189-60-8 79%
Reaction Conditions:
with potassium phosphate;bis(1,5-cyclooctadiene)nickel (0);bis(N-methylimidazol-2-yl)methane in N,N-dimethyl acetamide at 80; for 2 h;Product distribution / selectivity;Suzuki Coupling;
Steps:
16; 17 Examples 14 to 18
Examples 14 to 18 The process of Example 1 was repeated in a similar manner except that 0.40 mmol of phenylboronic acid was used in place of p-methoxyphenylboronic acid and that 1 ml of each solvent as shown in Table 2 was used in place of N,N-, dimethylacetamide. The result is shown in Table 2. [Table 2] Ex. NoSolventReaction TimeYield (%)14Tetrahydrofuran4hr5915Ethyleneglycol dimethyl ether↑6116N,N-dimethylacetamide2hr8717N,N-dimethylacetamide2hr7918Ethanol4hr48
References:
Sumitomo Chemical Co.,Ltd. EP1439157, 2004, A2 Location in patent:Page 12
1674-37-9
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2189-60-8
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629-27-6
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100-59-4
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2189-60-8
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$30.00/20mg
111-83-1
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$12.00/25g
603-35-0
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2189-60-8
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$30.00/20mg
6737-43-5
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