Trimethylsulfonium iodide synthesis
- Product Name:Trimethylsulfonium iodide
- CAS Number:2181-42-2
- Molecular formula:C3H9IS
- Molecular Weight:204.07
(CH3)2SO + CH3I → (CH3)3SO+I
75-18-3
396 suppliers
$18.10/8208330005
74-88-4
349 suppliers
$15.00/10g
2181-42-2
262 suppliers
$6.00/5g
Yield:2181-42-2 66%
Reaction Conditions:
at 25; for 15 h;
Steps:
Trimethylsulfonium iodide (3)
Dimethyl sulphide (1.2 mL, 16.1 mmol) and methyl iodide (1 mL, 16.1 mmol) were stirred at 25 °C for 15 hrs. The resulting precipitate was ground via mortar and pestle, recrystallised from EtOH and dried under reduced pressure to afford clear colourless crystals (2.16 g, 10.6 mmol, 66%);
References:
Ledingham, Edward T.;Merritt, Christopher J.;Sumby, Christopher J.;Taylor, Michelle K.;Greatrex, Ben W. [Synthesis,2017,vol. 49,# 12,p. 2652 - 2662] Location in patent:supporting information
75-18-3
396 suppliers
$18.10/8208330005
75-11-6
353 suppliers
$10.00/5g
2181-42-2
262 suppliers
$6.00/5g
74-88-4
349 suppliers
$15.00/10g
2181-42-2
262 suppliers
$6.00/5g
75-18-3
396 suppliers
$18.10/8208330005
2181-42-2
262 suppliers
$6.00/5g