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ChemicalBook CAS DataBase List Bromobenzene
108-86-1

Bromobenzene synthesis

13synthesis methods
Bromobenzene is obtained by reacting benzene with bromine. First add iron powder and benzene into the reactor, slowly add bromine under stirring, keep the reaction at 70-80°C for 1 h after adding, the obtained crude product is washed with water and 5% sodium hydroxide solution, left to stand for stratification, distillation, Drying, filtering, and finally fractional distillation under constant pressure, taking the fraction at 155-157°C to obtain the finished product.
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Yield:108-86-1 100%

Reaction Conditions:

with carbon dioxide;bromine at 40; under 187519 Torr; for 2 h;Supercritical conditions;Green chemistry;

References:

Delgado-Abad, Thais;Martnez-Ferrer, Jaime;Reig-Lpez, Javier;Mello, Rossella;Acerete, Rafael;Asensio, Gregorio;Gonzlez-Nez, Mara Elena [RSC Advances,2014,vol. 4,# 92,p. 51016 - 51021]

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