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ChemicalBook CAS DataBase List 4-(4-FLUORO-PHENYL)-PIPERIDIN-4-OL HYDROCHLORIDE
3888-65-1

4-(4-FLUORO-PHENYL)-PIPERIDIN-4-OL HYDROCHLORIDE synthesis

9synthesis methods
163631-02-5 Synthesis
1-BENZYL-4-(4-FLUOROPHENYL)PIPERIDIN-4-OL

163631-02-5
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Yield: 82%

Reaction Conditions:

with 10 wt% Pd(OH)2 on carbon;hydrogen in methanol

Steps:

I.1.12.2
To a solution of Compound 2 (0.9 g, 3.1 mmol) in MeOH was added Pd(OH)2/C (100 mg), and the formed mixture was stirred under H2 balloon overnight. The Pd was filtered and the filtrate was concentrated to give the desired product (0.5 g, 82 %). LCMS: 196.2 [M+l].

References:

NOVIRA THERAPEUTICS, INC.;HARTMAN, George D.;FLORES, Osvaldo A. WO2013/96744, 2013, A1 Location in patent:Page/Page column 213

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