ChemicalBook CAS DataBase List 3-NITROBENZANILIDE

3-NITROBENZANILIDE synthesis

14synthesis methods

Product Name:3-NITROBENZANILIDE
CAS Number:2243-73-4
Molecular formula:C13H10N2O3
Molecular Weight:242.23

645-00-1
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201230-82-2 Synthesis

201230-82-2
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62-53-3 Synthesis

62-53-3
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2243-73-4
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Yield:2243-73-4 100%

Reaction Conditions:

with triethylamine in N,N-dimethyl-formamide at 100; under 750.075 Torr; for 8 h;Schlenk technique;Inert atmosphere;

Steps:

2.3.2. Catalytic reactions at atmospheric pressure

General procedure: In a typical experiment a solution containing the palladiumcatalyst (with 6 mol Pd-content) was placed in a Schlenk-tube.Under argon, 0.2 mmol (22.5 l) iodobenzene (1), 0.5 mmol aminereagent, 0.7 mmol (100 l) triethylamine and 1 ml solvent wasadded and the atmosphere was changed to carbon monoxide. Thereaction mixture was heated with stirring in an oil bath at 100Cand was analysed by gas chromatography.

References:

Urbán, Béla;Papp, Máté;Srankó, Dávid;Skoda-F?ldes, Rita [Journal of Molecular Catalysis A: Chemical,2015,vol. 397,p. 150 - 157]

62-53-3 Synthesis

62-53-3
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