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3-ISOPROPYLPHENOL synthesis
- Product Name:3-ISOPROPYLPHENOL
- CAS Number:618-45-1
- Molecular formula:C9H12O
- Molecular Weight:136.19
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5369-16-4
111 suppliers
$9.00/1g
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618-45-1
100 suppliers
$67.00/5g
Yield:618-45-1 58%
Reaction Conditions:
with uranyl acetate monohydrate;water;trifluoroacetic acid in acetonitrile; for 48 h;Irradiation;Inert atmosphere;
Steps:
4 Example 4
In a 25mL reaction tube, add 3-isopropylaniline (0.2mmol, 27.0mg), water (0.6mmol, 10.8mg), uranyl acetate hydrate (4mol%/0.008mmol, 3.4mg), trifluoroacetic acid ( 0.2mmol, 22.8mg), acetonitrile (2mL), stirred for 2 days under the irradiation of a 6-watt blue LED lamp (wavelength 460nm) in a nitrogen atmosphere. After the reaction is complete, it is extracted, concentrated, and subjected to column chromatography (VPE/VEA=10/ 1) Isolated brown liquid 3d (15.8mg, 58%).
References:
CN112778125,2021,A Location in patent:Paragraph 0050-0053
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187737-37-7
1 suppliers
inquiry
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108-95-2
746 suppliers
$14.00/25g
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88-69-7
182 suppliers
$5.00/5G
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2934-05-6
82 suppliers
$20.00/100mg
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618-45-1
100 suppliers
$67.00/5g
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98-82-8
282 suppliers
$9.00/5ml
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88-69-7
182 suppliers
$5.00/5G
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617-94-7
196 suppliers
$6.00/1g
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618-45-1
100 suppliers
$67.00/5g