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ChemicalBook CAS DataBase List 2-Chlorobenzotrichloride
2136-89-2

2-Chlorobenzotrichloride synthesis

9synthesis methods
-

Yield:2136-89-2 91%

Steps:

IV Preparation of 2-Chlorobenzotrichloride
EXAMPLE IV Preparation of 2-Chlorobenzotrichloride 23.5 gms of 2-chlorobenzal chloride was reacted in accordance with the procedure of Example III and refluxed for 3 hours to give 25 gms of a pale yellow liquid. (Yield 91%). [Pot temperature 90° -110° C. (at 0.1 mm/Hg - 0.13-105 pascals)].

References:

Monsanto Company US4593144, 1986, A

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