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ChemicalBook CAS DataBase List 2-Chloro-N-(2,6-dimethylphenyl)acetamide
1131-01-7

2-Chloro-N-(2,6-dimethylphenyl)acetamide synthesis

9synthesis methods
-

Yield:1131-01-7 89%

Steps:

289.A 2-chloro-N-(2,6-dimethylphenyl)acetamide
EXAMPLE 289A 2-chloro-N-(2,6-dimethylphenyl)acetamide The procedure described in Example 22A was followed, substituting 2,6-dimethylphenylamine for 3,4,5-trimethoxyaniline to provide the title compound (7.21 g, 89%) 1H NMR (300 MHz, CDCl3) δ 2.25 (s, 6H), 4.26 (s, 2H), 6.65 (t, J=7.46 Hz, 1H, 6.95 (d, J=7.46 Hz, 2H), 7.84 (s, 3H); MS (ESI) m/e 198 (M+H)+.

References:

Bhatia, Pramila A.;Daanen, Jerome F.;Hakeem, Ahmed A.;Kolasa, Teodozyj;Matulenko, Mark A.;Mortell, Kathleen H.;Patel, Meena V.;Stewart, Andrew O.;Wang, Xueqing;Xia, Zhiren;Zhang, Henry Q. US2004/29887, 2004, A1

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