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N-Phenyl-bis(trifluoromethanesulfonimide)

N-Phenyl-bis(trifluoromethanesulfonimide) Struktur
37595-74-7
CAS-Nr.
37595-74-7
Englisch Name:
N-Phenyl-bis(trifluoromethanesulfonimide)
Synonyma:
PHENYL TRIFLIMIDE;N,N-BIS(TRIFLUOROMETHYLSULFONYL)ANILINE;N-PHENYLBIS(TRIFLUOROMETHANESULFONIMIDE);1,1,1-trifluoro-N-phenyl-N-trifluoromethanesulfonylmethanesulfonamide;N-PHENYLTRIFLUOROMETHANESULFONIMIDE;phenyltrifluoromethanesulfonimide;N-PHENYLBIS(TRIFLUOROMETHANESULPHONIMIDE);trifluoro-N-phenyl-N-(trifluoromethylsulfonyl)methanesulfonamide;N-PHENYLT;NSC 240874
CBNumber:
CB5289550
Summenformel:
C8H5F6NO4S2
Molgewicht:
357.25
MOL-Datei:
37595-74-7.mol

N-Phenyl-bis(trifluoromethanesulfonimide) Eigenschaften

Schmelzpunkt:
100-102 °C(lit.)
Siedepunkt:
305.3±52.0 °C(Predicted)
Dichte
1.766±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
L?slichkeit
Soluble in methanol. Slightly soluble in chloroform and ethyl acetate.
pka
-13.12±0.50(Predicted)
Aggregatzustand
Crystals or Crystalline Powder
Farbe
White or colorless
Sensitive 
Moisture Sensitive
BRN 
1269141
Stabilit?t:
Moisture Sensitive
InChI
InChI=1S/C8H5F6NO4S2/c9-7(10,11)20(16,17)15(6-4-2-1-3-5-6)21(18,19)8(12,13)14/h1-5H
InChIKey
DIOHEXPTUTVCNX-UHFFFAOYSA-N
SMILES
C(F)(F)(F)S(N(C1=CC=CC=C1)S(C(F)(F)F)(=O)=O)(=O)=O
CAS Datenbank
37595-74-7(CAS DataBase Reference)
NIST chemische Informationen
N-phenyltrifluoromethanesulfonimide(37595-74-7)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher Xi
R-S?tze: 36/37/38
S-S?tze: 26-36
WGK Germany  3
F  21
TSCA  No
HazardClass  IRRITANT
HS Code  29242100
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizit?t (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" />
Sicherheit
P261 Einatmen von Staub vermeiden.
P264 Nach Gebrauch gründlich waschen.
P264 Nach Gebrauch gründlich waschen.
P271 Nur im Freien oder in gut belüfteten R?umen verwenden.
P280 Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.
P302+P352 BEI BERüHRUNG MIT DER HAUT: Mit viel Wasser/... (Hersteller kann, falls zweckm??ig, ein Reinigungsmittel angeben oder, wenn Wasser eindeutig ungeeignet ist, ein alternatives Mittel empfehlen) waschen.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

N-Phenyl-bis(trifluoromethanesulfonimide) Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.

S-S?tze Betriebsanweisung:

S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.
S36:DE: Bei der Arbeit geeignete Schutzkleidung tragen.

Beschreibung

N-Phenylbis(trifluoromethanesulfonimide) acts as a mild triflating reagent as well as a transparent strong electron-withdrawing p-type dopant in carbon nanotubes. It is also employed as a reactant for the preparation of amphoteric alfa-boryl aldehydes. It plays an important role in the enantioselective synthesis of the core ring skeleton of leucosceptroids A-D and in steroselective sulfoxidation. 

Chemische Eigenschaften

white to off-white crystalline powder

Synthese

Add methylene chloride, aniline, 4-dimethylaminopyridine (DMAP), and triethylamine to a reactor equipped with a thermometer, distillation device, and mechanical stirring. When the vacuum of the reactor is evacuated to -0.095MPa and cooled to -40°C, trifluoromethanesulfonyl fluoride gas is introduced and then stirred at -20°C ~ 0°C and 0.02MPa ~ 0.1MPa reaction pressure, and react for 6 hours Finally, the excess trifluoromethanesulfonyl fluoride gas in the reactor is released and collected by cooling. After the inside of the reactor is brought to normal pressure, 500 mL of water is added, and the liquid is separated. A light yellow solid is obtained after the organic phase is heated to 40°C and methylene chloride is distilled. The light yellow solid is recrystallized with toluene to obtain 650g of white crystal N-Phenyl-bis(trifluoromethanesulfonimide).

N-Phenyl-bis(trifluoromethanesulfonimide) Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Natriumhydrid Ethanol Natriumchlorid Trifluormethansulfonylchlorid Kaliumcarbonat Trifluormethansulfonsaeureanhydrid N,N-Diethylethanamin Tetrahydrofuran Anilin Dichlormethan Natriumhydroxid Magnesiumsulfat

Downstream Produkte

1-Boc-4-methanesulfonyloxypiperidine 2-(triMethylsilyl)ethyl 4-(trifluoroMethylsulfonyloxy)-5,6-dihydropyridine-1(2H)-carboxylate 1-CYCLOHEXEN-1-YL TRIFLUOROMETHANE- Methyl 3-((Trifluoromethylsulfonyl)oxy)phenylacetate

N-Phenyl-bis(trifluoromethanesulfonimide) Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 510)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
JIANGXI TIME PHARMACEUTICAL CO.,LTD 		+86-0794-7183888 +86-13155888520
 sales@groupchem.com China 27 58
Fluoropharm Co., Ltd. 		+86-0571-85586753; +8613336034509
 sales@fluoropharm.com China 1376 60
SHANGHAI T&W PHARMACEUTICAL CO., LTD.
+86-021-61551413 +8618813727289
 contact@trustwe.com China 5738 58
Hebei Mojin Biotechnology Co., Ltd 		+86 13288715578 +8613288715578
 sales@hbmojin.com China 12825 58
Hebei Weibang Biotechnology Co., Ltd 		+8617732866630
 bess@weibangbio.com China 18275 58
Zibo Hangyu Biotechnology Development Co., Ltd 		+86-0533-2185556 +8617865335152
 Mandy@hangyubiotech.com China 10986 58
Capot Chemical Co.,Ltd. 		+86-（0）57185586718 +86-13336195806
 sales@capot.com China 29791 60
Shanghai Daken Advanced Materials Co.,Ltd 		+86-371-66670886
info@dakenam.com China 18648 58
Beijing Cooperate Pharmaceutical Co.,Ltd 		010-60279497
sales01@cooperate-pharm.com CHINA 1803 55
Henan Tianfu Chemical Co.,Ltd. 		+86-0371-55170693 +86-19937530512
 info@tianfuchem.com China 21639 55

37595-74-7()Verwandte Suche:

  • 1,1,1-TRIFLUORO-N-PHENYL-N-[(TRIFLUOROMETHYL)SULFONYL]METHANESULFONAMIDE
  • N-Phenylbis(trifluoromethanesulphonimide), Phenyl triflimide
  • N-Phenyl bis trifluorosulphonamide
  • N-Bis(trifluoromethylsulfonyl)aniline
  • 1,1,1-trifluoro-N-(methylsulfonyl)methanesulfonamide
  • N- phenyl-bis (trifluoromethanesulfonyl) imide
  • N-Phenylbis(trifluoroMethanesulfoniMide), 97% 5GR
  • N,N-Bis(trifluoromethylsulfonyl)aniline Phenyl Triflimide N-Phenyltrifluoromethanesulfonimide
  • N,N-Bis(trifluoroMethylsufonyl)aniline
  • N,N-Bis(trifluoroMethylsulfonyl)aniline SynonyMs N-Phenylbis(trifluoroMethanesulfon)iMide
  • N-phenyldouble(threefluoro Methanesulfonic acidiMide
  • N-Phenyl-bis(trifluoroMethanesulfoniMide) >=98.0% (HPLC)
  • N,N-Bis(trifluoromethanesulphonyl)aniline~Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide
  • Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide
  • N-PHENYL-BIS-(TRIFLUORMETHANSULFONIMID)
  • N,N-BIS-(TRIFLUOROMETHANESULFONYL)ANILINE
  • 1,1,1-Trifluoro-N-phenyl-N-(trifluoromethyl)sulphonylmethanesulphonamide
  • n-phenylbis(trifluorometanesulfonimide)
  • N-Phenyl-bis(trifluoromethyl)sulfonimide
  • N-Phenylbis(trifluoromethanesulfonimide) [Triflating Reagent]
  • N-phenyl-bis(trifluoromethanesulfonamide)
  • N,N-Bis(trifluoromethylsulfonyl)aniline, N-Phenyl-trifluoromethanesulfonimide, Phenyl triflimide, 1,1,1-Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide
  • N-Phenyltrifluoromethanesulfonimide ,98%
  • N-Phenyl-bis(trifluoromethanesulfonimide),1,1,1-Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide, N,N-Bis(trifluoromethylsulfonyl)aniline, N-Phenyl-trifluoromethanesulfonimide, Pheny
  • N,N-Bis(trifluoromethylsulphonyl)aniline 98%
  • N-Phenylbis(trifluoromethanesulfonyl)amine
  • N-Phenylbis(trifluoromethylsulfonyl)amine
  • N-Phenyl-N,N-bis(trifluoromethylsulfonyl)amine
  • N-Phenylbis(trifluoromethanesulphonimide)97%
  • N-Phenylbis(trifluoromethanesulfonimide),97%
  • N-Phenylbis(trifluromethanesulphonimide)99%
  • N-phenyl bis(trifluoromethanesulfonyl)amide
  • N-Phenyl-bis(trifluoromethanesulfonimide) 37595-74-7
  • N,N-Bis(trifluoromethylsulfonyl)aniline 37595-74-7
  • -bis(trifL
  • fonimide)
  • N-Phenylbis(trifluoromethanesulfonimide)[TriflatingReagent]>
  • Methanesulfonamide, 1,1,1-trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]-
  • 1,1,1-trifluoro-N-phenyl-N
  • TIANFUCHEM--37595-74-7--N-Phenyl-bis(trifluoromethanesulfonimide) factory price
  • phenyltrifluoromethanesulfonimide
  • N-PHENYLBIS(TRIFLUOROMETHANESULFONIMIDE)
  • N-PHENYLBIS(TRIFLUOROMETHANESULPHONIMIDE)
  • N-PHENYLTRIFLUOROMETHANESULFONIMIDE
  • N-PHENYLTRIFLUOROMETHANESULPHONIMIDE
  • N,N-BIS(TRIFLUOROMETHYLSULFONYL)ANILINE
  • NSC 240874
  • 1,1,1-trifluoro-N-phenyl-N-trifluoromethanesulfonylmethanesulfonamide
  • PHENYL TRIFLIMIDE
  • trifluoro-N-phenyl-N-(trifluoromethylsulfonyl)methanesulfonamide
  • N-PHENYLT
  • Bis(trifluoromethylsulfonyl)aniline
  • N- phenylbis (trifluoromethanesulfonyl) imine
  • N-PHENYL-BIS(TRIFLUROMETHANSULPHONIMIDE)
  • N-phenylbis (trifluoromesulfonimide)
  • 37595-74-7
  • 7595-74-7
  • 37595-74-4
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