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ChemicalBook--->CAS DataBase List--->6011-14-9

6011-14-9

6011-14-9 Structure

6011-14-9 Structure
IdentificationMore
[Name]

Aminoacetonitrile hydrochloride
[CAS]

6011-14-9
[Synonyms]

AMINO ACETONITRILE HCL
AMINOACETONITRILE HYDROCHLORIDE
Glycinonitrile hydrochloride
alpha-aminoacetonitrilehydrochloride
aminoacetonitrilemonohydrochloride
amino-acetonitrilmonohydrochloride
glycinonitrile,monohydrochloride
2-AminoacetonitrileHydrochloride
GlycinonitrileHCl
Aminoacetonitrilehydrochloride,97%
Acetonitrile, amino-, monohydrochloride
AMINOACETONITRILE A.K.A. GLYCINONITRILE HYDROCHLOR
Aminoacetonitrile hydrochloride, 98+%
Cyanomethylazanium chloride
[EINECS(EC#)]

227-865-9
[Molecular Formula]

C2H5ClN2
[MDL Number]

MFCD00012850
[Molecular Weight]

92.53
[MOL File]

6011-14-9.mol
Chemical PropertiesBack Directory
[Melting point ]

172-174°C
[RTECS ]

MC1950000
[storage temp. ]

Inert atmosphere,Room Temperature
[solubility ]

Methanol (Slightly, Heated), Water
[form ]

Powder
[color ]

White to Off-White
[Water Solubility ]

Soluble in water 20°C, 1000g/L.
[Sensitive ]

Hygroscopic
[Detection Methods]

NMR,T
[Merck ]

14,412
[CAS DataBase Reference]

6011-14-9(CAS DataBase Reference)
[Storage Precautions]

Moisture sensitive
[EPA Substance Registry System]

6011-14-9(EPA Substance)
Safety DataBack Directory
[Risk Statements ]

R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S22:Do not breathe dust .
S36/37:Wear suitable protective clothing and gloves .
[RIDADR ]

3439
[TSCA ]

Yes
[HazardClass ]

6.1
[PackingGroup ]

III
[HS Code ]

29269090
[Safety Profile]

An experimental teratogen. Experimental reproductive effects. When heated to decomposition it emits toxic fumes of NOx and HCl.
Raw materials And Preparation ProductsBack Directory
[Preparation Products]

1-AMINOCYCLOPROPANECARBONITRILE-->2-AMINOPENT-4-YNENITRILE-->Momelotinib-->3-Indoleacetonitrile-->(4-FLUOROPHENYLTHIO)ACETONITRILE-->N-(tert-Butoxycarbonyl)-2-aminoacetonitrile-->4-Biphenylacetonitrile-->2-Methylbenzyl cyanide-->Acetonitrile, 2-isothiocyanato--->N-(CYANOMETHYL)-4-METHYLBENZAMIDE-->N-(CYANOMETHYL)ACETAMIDE-->3,4-Dichlorophenylacetonitrile
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

Aminoacetonitrile hydrochloride(6011-14-9).msds
Hazard InformationBack Directory
[Chemical Properties]

White to light brown solid
[Uses]

Used as pharmaceutical intermediates, organic synthetic raw material transportation.
[Application]

Aminoacetonitrile is a useful synthetic intermediate. It is a reagent used to synthesize dipeptide nitriles as reversible and potent cathepsin S inhibitors. It can also used to prepare substituted cyclic ureas as possible HIV protease inhibitors.
[Preparation]

Synthesis of Aminoacetonitrile Hydrochloride by Reaction of Aminoacetonitrile with Hydrogen Chloride in Methanol: mixing the aminoacetonitrile with hydrogen chloride methanol solution, reacting at 45-50°C for 1-2 hours, cooling to below 5°C, filtering, and centrifugalizing to obtain the aminoacetonitrile hydrochloride, wherein in the hydrogen chloride methanol solution, the content of hydrogen chloride is 30-50 wt%, and the water content is less than or equal to 1%.
Preparation method of aminoacetonitrile hydrochloride
[Purification Methods]

The salt recrystallises from dilute EtOH as hygroscopic leaflets. It is best to crystallise it from absolute EtOH/Et2O (1:1) and then recrystallise it from absolute EtOH. The melting point recorded ranges from 144o to 174o. The free base has b 58o/15mm with partial decomposition. [Klages J Prakt Chem [2] 65 189 1902, Mange J Am Chem Soc 56 2197 1934, Goldberg & Kelly J Chem Soc 1371 1947, Beilstein 4 H 344, 4 I 468, 4 II 783, 4 III 1120, 4 IV 2363.]
Spectrum DetailBack Directory
[Spectrum Detail]

Aminoacetonitrile hydrochloride(6011-14-9)1HNMR
Aminoacetonitrile hydrochloride(6011-14-9)IR1
Aminoacetonitrile hydrochloride(6011-14-9)IR2
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

Aminoacetonitrile hydrochloride, 98+%(6011-14-9)
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