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ChemicalBook--->CAS DataBase List--->1072-98-6

1072-98-6

1072-98-6 Structure

1072-98-6 Structure
IdentificationMore
[Name]

2-Amino-5-chloropyridine
[CAS]

1072-98-6
[Synonyms]

2-AMINO-5-CHLOROPYRIDINE
5-CHLORO-2-AMINOPYRIDINE
5-CHLORO-2-PYRIDINAMINE
5-CHLORO-2-PYRIDYLAMINE
5-CHLORO-A-PYRIDYLAMINE
5-CHLOROPYRIDIN-2-AMINE
5-CHLOROPYRIDIN-2-YLAMINE
AKOS 91155
AMINO(2-)-5-CHLOROPYRIDINE
TIMTEC-BB SBB000059
2-Pyridinamine, 5-chloro-
Pyridine, 2-amino-5-chloro-
2-Amino-5-Chloro Pyriine
2-AMINO-5-CHLOROPYRIDINE 99%
2-AMINO-5-CHLIROPYRIDINE
2-Pyridinamine,5-chloro-(9CI)
2-Amino-5-chloropyridine 
2-Amino-5-chloropyridine
2-AMINO-5-CHLOROPYRIDINE 5-CHLORO-PYRIDIN-2-YLAMINE
5-Chloro-2-pyridineamine
[EINECS(EC#)]

214-020-4
[Molecular Formula]

C5H5ClN2
[MDL Number]

MFCD00006324
[Molecular Weight]

128.56
[MOL File]

1072-98-6.mol
Chemical PropertiesBack Directory
[Appearance]

beige to beige-brown crystalline powder
[Melting point ]

135-138 °C (lit.)
[Boiling point ]

127-128 °C/11 mmHg (lit.)
[density ]

1.2417 (rough estimate)
[refractive index ]

1.5110 (estimate)
[Fp ]

160 °C
[storage temp. ]

2-8°C
[solubility ]

1.0g/l
[form ]

Crystalline Powder
[pka]

4.67±0.13(Predicted)
[color ]

Beige to beige-brown
[Water Solubility ]

1 g/L (20 ºC)
[Detection Methods]

HPLC,NMR
[BRN ]

108735
[InChIKey]

MAXBVGJEFDMHNV-UHFFFAOYSA-N
[CAS DataBase Reference]

1072-98-6(CAS DataBase Reference)
[NIST Chemistry Reference]

2-Amino-5-chloropyridine(1072-98-6)
[EPA Substance Registry System]

1072-98-6(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R22:Harmful if swallowed.
R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
S37/39:Wear suitable gloves and eye/face protection .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[Hazard Note ]

Harmful
[HazardClass ]

IRRITANT
[HS Code ]

29333999
Raw materials And Preparation ProductsBack Directory
[Preparation Products]

Zopiclone-->2,5-Dichloropyridin-3-amine-->2,5-Dichloro-3-nitropyridine-->5-Chloro-2-hydroxy-3-nitropyridine-->ethyl 2-(6-aminopyridin-3-yl)acetate-->6-chloro-[1,2,4]triazolo[1,5-a]pyridin-2-amine-->EthanediaMide iMpurity F-->2-Bromo-5-chloropyridine-->2-Bromo-5-chloro-3-nitropyridine-->2-Amino-5-chloro-3-nitropyridine-->3-AMINO-2-BROMO-5-CHLOROPYRIDINE-->5-Chloropyridine-2-carboxylic acid
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

2-Amino-5-chloropyridine(1072-98-6).msds
Hazard InformationBack Directory
[Chemical Properties]

beige to beige-brown crystalline powder
[Uses]

5-Chloro-2-pyridinamine is a useful synthetic intermediate. It can be used to synthesize zopiclone (Z700500) which is a cyclopyrrolone member of a family of non-benzodiazepine GABAA receptor agonists.
[Synthesis Reference(s)]

The Journal of Organic Chemistry, 41, p. 93, 1976 DOI: 10.1021/jo00863a020
[Purification Methods]

Recrystallise this base from pet ether. It sublimes at 50o/0.5mm. [Beilstein 22 II 332, 22/8 V 541.]
Spectrum DetailBack Directory
[Spectrum Detail]

2-Amino-5-chloropyridine(1072-98-6)MS
2-Amino-5-chloropyridine(1072-98-6)1HNMR
2-Amino-5-chloropyridine(1072-98-6)13CNMR
2-Amino-5-chloropyridine(1072-98-6)IR1
2-Amino-5-chloropyridine(1072-98-6)IR2
2-Amino-5-chloropyridine(1072-98-6)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

2-Amino-5-chloropyridine, 98%(1072-98-6)
[Alfa Aesar]

2-Amino-5-chloropyridine, 98%(1072-98-6)
[Sigma Aldrich]

1072-98-6(sigmaaldrich)
[TCI AMERICA]

2-Amino-5-chloropyridine,>98.0%(GC)(T)(1072-98-6)
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