VINYLCYCLOHEXANE synthesis
- Product Name:VINYLCYCLOHEXANE
- CAS Number:695-12-5
- Molecular formula:C8H14
- Molecular Weight:110.2
1193-81-3
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695-12-5
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1003-64-1
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Yield:-
Reaction Conditions:
5 % ruthenium on Al2O3;zirconium(IV) oxide at 376 - 398;Product distribution / selectivity;
Steps:
2.3.C
(3) Step (C)To a tubular reactor made of metal (having a sectional area of 4.1 square centimeter) was packed 41 grams of a zirconium oxide catalyst (packed length: 10 cm), and then the hydrogenation catalyst-removed liquid obtained in the above (2) was fed in 320 g/hour and the temperature of the zirconium oxide catalyst layer was adjusted to 376 to 398° C.The conversion of 1-cyclohexylethanol at the reactor outlet was 45%, the selectivity of vinylcyclohexane was 84%, and the selectivity of ethylidenecyclohexane, which is a by-product, was 6%.
References:
SUMITOMO CHEMICAL COMPANY, LIMITED US2012/165587, 2012, A1 Location in patent:Page/Page column 5
931-48-6
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695-12-5
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$53.00/5mL
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81372-29-4
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695-12-5
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5664-20-0
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695-12-5
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1003-64-1
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$139.00/10g
24371-94-6
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695-12-5
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