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ChemicalBook CAS DataBase List SUCCINALDEHYDIC ACID
692-29-5

SUCCINALDEHYDIC ACID synthesis

12synthesis methods
-

Yield:108-30-5 60 %Spectr. ，692-29-5 17 %Spectr.

Reaction Conditions:

with Aeroxide (Evonik) P25 TiO2, consisting of a 3:1 anatase/rutile mixture in methanol;acetonitrile for 15 h;Inert atmosphere;UV-irradiation;

Steps:

3.3. General Procedure for SCPC Hydrogenation of Maleimides
General procedure: The maleimide was added to a suspension of P25 in methanol (10%) and acetonitrile (90%). The resulting mixture was then purged with argon for 15 min. The mixture was irradiated with eight 29 cm 15 W Philips Cleo tubes (λ = 350 nm). Following irradiation the P25 powder was removed via filtration through Celite.

References:

Manley, David W.;Buzzetti, Luca;MacKessack-Leitch, Andrew;Walton, John C. [Molecules,2014,vol. 19,# 9,p. 15324 - 15338]

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