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ChemicalBook CAS DataBase List MELLITIC ACID
517-60-2

MELLITIC ACID synthesis

7synthesis methods
-

Yield:517-60-2 54%

Reaction Conditions:

Stage #1:1,2,3,4,5,6-cyclohexanehexacarboxylic acid with phosphorus pentachloride in neat (no solvent) at 130; for 1 h;
Stage #2: with water in neat (no solvent) at 130; for 4 h;

References:

Geraskina, Margarita R.;Juetten, Mark J.;Winter, Arthur H. [Journal of Organic Chemistry,2014,vol. 79,# 11,p. 5334 - 5337]

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