Ethylene Glycol Dibutyl Ether synthesis
- Product Name:Ethylene Glycol Dibutyl Ether
- CAS Number:112-48-1
- Molecular formula:C10H22O2
- Molecular Weight:174.28
107-21-1
1365 suppliers
$10.00/25g
123-72-8
433 suppliers
$12.32/25ML
111-76-2
768 suppliers
$9.00/1g
112-48-1
175 suppliers
$7.00/5g
71-36-3
1071 suppliers
$14.00/25mL
Yield:111-76-2 79.7 %Chromat. ，112-48-1 7.7 %Chromat. ，71-36-3 7.5 %Chromat.
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon at 180; under 51716.2 Torr; for 2 h;Product distribution / selectivity;Inert atmosphere;
Steps:
5
In Examples 1-10, n-butyraldehyde, ethylene glycol, and hydrogen are reacted in the presence of Pd/C at various ratios and/or reaction conditions. The reaction procedure is generally as follows. The n-butyraldehyde, ethylene glycol, and Pd/C are charged to a Parr reactor. The system is purged with nitrogen three times. Then hydrogen is charged, the reactor is heated, and the hydrogen pressure is adjusted as necessary. Following the appropriate reaction time, the product mixture is analyzed by GC. Reaction conditions and GC results are summarized in Table 1.
References:
US2010/48940,2010,A1 Location in patent:Page/Page column 6-7
107-21-1
1365 suppliers
$10.00/25g
123-72-8
433 suppliers
$12.32/25ML
3390-13-4
9 suppliers
$90.00/500mg
111-76-2
768 suppliers
$9.00/1g
112-48-1
175 suppliers
$7.00/5g
71-36-3
1071 suppliers
$14.00/25mL
2351-69-1
27 suppliers
inquiry
112-48-1
175 suppliers
$7.00/5g