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85539-84-0

ETHYL BROMOACETATE-2-13C synthesis

4synthesis methods
-

Yield:85539-84-0 93%

Reaction Conditions:

Stage #1: (2-13C)bromoacetic acidwith oxalyl dichloride at 20; for 30 h;
Stage #2: ethanol at 20; for 0.5 h;Further stages.;

References:

Creemers, Alain F. L.;Lugtenburg, Johan [Journal of the American Chemical Society,2002,vol. 124,# 22,p. 6324 - 6334]

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