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ChemicalBook CAS DataBase List Dimethyl itaconate
617-52-7

Dimethyl itaconate synthesis

7synthesis methods
-

Yield:617-52-7 93.07%

Reaction Conditions:

with La3+SO42-/TiO2-SiO2 at 120; for 7 h;Autoclave;Reagent/catalyst;Time;Concentration;

Steps:

Esterification of itaconic acid with methanol
A mixture of itaconic acid, methanol and catalyst was put into 100 mL autoclave and stirred at 120 °C. Various parameters, such as the molar ratio of methanol to itaconic acid, amount of catalyst, and reaction time, were varied to optimize the reaction conditions. After the reaction, catalyst was separated by filtering

References:

Li, Lu;Liu, Shiwei;Xu, Junming;Yu, Shitao;Liu, Fusheng;Xie, Congxia;Ge, Xiaoping;Ren, Jianyun [Journal of Molecular Catalysis A: Chemical,2013,vol. 368-369,p. 24 - 30]

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