ChemicalBook CAS DataBase List Diethyl oxalate

Diethyl oxalate synthesis

13synthesis methods

Product Name:Diethyl oxalate
CAS Number:95-92-1
Molecular formula:C6H10O4
Molecular Weight:146.14

Diethyl oxalate is produced via esterification of ethanol and oxalic acid. It is a preferred solvent for cellulose acetate and nitrate.

64-17-5 Synthesis

64-17-5
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$10.00/50g

144-62-7 Synthesis

144-62-7
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$5.00/5g

95-92-1
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Yield:95-92-1 99.3%

Reaction Conditions:

with enriched hydroxylated graphene oxide in benzene at 120 - 140;

Steps:

4 Example 4

Example 4 400 ml of 98% sulfuric acid was maintained at a temperature of -2 ° C,Add 10 ml of 30% hydrogen peroxide,After incubation for 30 min,Followed by adding 0.6g graphite powder,3.6g sodium perchlorate;Then 20 insulation 1-3h,Centrifugation to obtain hydroxylated graphene oxide;In 1000ml four bottles,Respectively, put oxalic acid,Ethanol,benzene,200 g of enriched graphene oxide, 220 g, 20 g, 1 g,The reaction temperature is controlled atBelow 120 ,Until there is no water out,Continue to heat up to 140 ° C,Distilled benzene,The benzene is distilled off.Cooling the separation of diethyl oxalate,Hydroxylated graphene oxide,The yield of diethyl oxalate was 99.3%.

References:

CN106542997,2017,A Location in patent:Paragraph 0013-0022

64-17-5 Synthesis

64-17-5
729 suppliers
$10.00/50g

201230-82-2 Synthesis