Decyl methacrylate synthesis
- Product Name:Decyl methacrylate
- CAS Number:3179-47-3
- Molecular formula:C14H26O2
- Molecular Weight:226.35
Yield: 100%
Reaction Conditions:
with sulfuric acid at 20; for 48 h;
Steps:
Synthesis of decyl methacrylate monomer (9)
Monomer 9 was synthesised following a previously publishedmethod (Yildiz et al., 2011). 250 mg of methacrylic acid 4(2.9 mmol), were added to 5 ml of 1-decanol 8 and sulfuric acidin catalytic amounts. The solution was stirred for 48 h at roomtemperature. After reaction the mixture was purified by silica gelchromatography eluting with Exane/EtOAc, gradient from 100%Exane to 95:5 to give compound 9 in quantitative yield.
References:
Martin, Chloe;Marino, Nino;Curran, Ciara;McHale, Anthony P.;Callan, John F.;Callan, Bridgeen [International Journal of Pharmaceutics,2016,vol. 511,# 1,p. 570 - 578]
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