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ChemicalBook CAS DataBase List Butyl methacrylate
97-88-1

Butyl methacrylate synthesis

14synthesis methods
n-Butyl methacrylate is produced by the reaction of methacrylic acid or methyl methacrylate with butanol .
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Yield:97-88-1 92.11%

Reaction Conditions:

with titanium catalyst at 115; for 1 h;

Steps:

3

2000 ppm of the titanium compound prepared in Synthesis Example 1 was put into the reactor,A mixture of methyl methacrylate and n-butanol in a ratio of 1.5: 1 was air-blown at 115 ° C,And reacted for 1 hour to prepare a methacrylic acid ester. A methacrylic acid ester was prepared by reacting in the same manner as in Example 1 except that methacrylic acid was used instead of methylmethacrylate.

References:

KR2016/67017,2016,A Location in patent:Paragraph 0045; 0048; 0049

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