Allyl methyl carbonate synthesis
- Product Name:Allyl methyl carbonate
- CAS Number:35466-83-2
- Molecular formula:C5H8O3
- Molecular Weight:116.12
616-38-6
690 suppliers
$5.00/5 g
35466-83-2
131 suppliers
$16.00/5g
Yield:-
Reaction Conditions:
potassium carbonate
Steps:
67 Synthesis of allyl methyl carbonate
Example 67 Synthesis of allyl methyl carbonate 422 g (7.27 mol) of allyl alcohol, 2120 g (23.6 mol) of dimethyl carbonate and 1.0 g (7.3 mmol) of potassium carbonate as a catalyst were charged into a 5 lit. four-necked flask and reacted at 90°C for 10 hr under reflux under agitation with removing formed methanol. After the completion of the reaction, potassium carbonate was removed by the use of a short column of silica gel, and then distillation was performed, thereby obtaining allyl methyl carbonate.
References:
MITSUI PETROCHEMICAL INDUSTRIES, LTD. EP787749, 1997, A1
107-18-6
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79-22-1
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35466-83-2
131 suppliers
$16.00/5g
107-18-6
2 suppliers
$24.60/100ml
616-38-6
690 suppliers
$5.00/5 g
35466-83-2
131 suppliers
$16.00/5g
107-18-6
2 suppliers
$24.60/100ml
616-38-6
690 suppliers
$5.00/5 g
35466-83-2
131 suppliers
$16.00/5g
15022-08-9
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$50.89/5g
67-56-1
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15022-08-9
65 suppliers
$50.89/5g
35466-83-2
131 suppliers
$16.00/5g