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6303-88-4

9-METHYL-2,3,4,9-TETRAHYDRO-1H-CARBAZOLE synthesis

13synthesis methods
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Yield:6303-88-4 97%

Reaction Conditions:

Stage #1: 1,2,3,4-tetrahydrocarbazolewith sodium hydride in tetrahydrofuran;mineral oil at 0 - 20; for 1 h;Inert atmosphere;Schlenk technique;Glovebox;
Stage #2: methyl iodide in tetrahydrofuran;mineral oil at 0 - 20; for 1 h;Inert atmosphere;Schlenk technique;Glovebox;

References:

Maier, Alexander F. G.;Tussing, Sebastian;Schneider, Tobias;Fl?rke, Ulrich;Qu, Zheng -Wang;Grimme, Stefan;Paradies, Jan [Angewandte Chemie - International Edition,2016,vol. 55,# 40,p. 12219 - 12223][Angew. Chem.,2016,vol. 128,p. 12407 - 12411] Location in patent:supporting information

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