ChemicalBook CAS DataBase List N-BENZYL-1,2,3,4-TETRAHYDROCARBAZOLE

N-BENZYL-1,2,3,4-TETRAHYDROCARBAZOLE synthesis

9synthesis methods

Product Name:N-BENZYL-1,2,3,4-TETRAHYDROCARBAZOLE
CAS Number:17017-63-9
Molecular formula:C19H19N
Molecular Weight:261.36

942-01-8 Synthesis

942-01-8
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100-39-0
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17017-63-9
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Yield:17017-63-9 128 mg

Reaction Conditions:

Stage #1: 1,2,3,4-tetrahydrocarbazolewith sodium hydride in tetrahydrofuran;N,N-dimethyl-formamide;mineral oil at 80; for 0.0833333 h;Microwave irradiation;
Stage #2: benzyl bromide in tetrahydrofuran;N,N-dimethyl-formamide;mineral oil at 80; for 0.5 h;Microwave irradiation;regioselective reaction;

References:

Hughes-Whiffing, Christopher A.;Perry, Alexis [Organic and Biomolecular Chemistry,2021,vol. 19,# 3,p. 627 - 634] Location in patent:supporting information