5-(4 4 5 5-TETRAMETHYL-1 3 2-DIOXABOROL& synthesis
- Product Name:5-(4 4 5 5-TETRAMETHYL-1 3 2-DIOXABOROL&
- CAS Number:479719-88-5
- Molecular formula:C14H17BO2S2
- Molecular Weight:292.22
61676-62-8
314 suppliers
$11.19/5G
492-97-7
316 suppliers
$5.00/1g
479719-88-5
91 suppliers
$21.00/100mg
Yield:479719-88-5 94%
Reaction Conditions:
Stage #1: 2,2'-Bithiophenewith n-butyllithium in tetrahydrofuran at -78 - 20; for 1.58333 h;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane at -78 - 20;
References:
Haid, Stefan;Marszalek, Magdalena;Mishra, Amaresh;Wielopolski, Mateusz;Teuscher, Joel;Moser, Jacques-E.;Humphry-Baker, Robin;Zakeeruddin, Shaik M.;Graetzel, Michael;Baeuerle, Peter [Advanced Functional Materials,2012,vol. 22,# 6,p. 1291 - 1302] Location in patent:experimental part
76-09-5
381 suppliers
$10.00/1g
492-97-7
316 suppliers
$5.00/1g
479719-88-5
91 suppliers
$21.00/100mg
61676-62-8
314 suppliers
$11.19/5G
3480-11-3
72 suppliers
$11.00/100mg
479719-88-5
91 suppliers
$21.00/100mg
3437-95-4
241 suppliers
$6.00/5g
1408285-51-7
1 suppliers
inquiry
479719-88-5
91 suppliers
$21.00/100mg
492-97-7
316 suppliers
$5.00/1g
25015-63-8
219 suppliers
$22.39/5G
479719-88-5
91 suppliers
$21.00/100mg