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ChemicalBook CAS DataBase List 4,N-DIMETHOXY-N-METHYLBENZAMIDE
52898-49-4

4,N-DIMETHOXY-N-METHYLBENZAMIDE synthesis

13synthesis methods
-

Yield:52898-49-4 100%

Reaction Conditions:

Stage #1: 4-methoxybenzoic acidwith oxalyl dichloride in dichloromethane;N,N-dimethyl-formamide at 0;
Stage #2: N,O-dimethylhydroxylamine*hydrochloridewith triethylamine in dichloromethane;N,N-dimethyl-formamide at 20;Further stages.;

References:

Bourne, Caryl;Roy, Sucharita;Wiley, Jenny L.;Martin, Billy R.;Thomas, Brian F.;Mahadevan, Anu;Razdan, Raj K. [Bioorganic and Medicinal Chemistry,2007,vol. 15,# 24,p. 7850 - 7864]

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