4,4'-DIMETHOXYBENZIL synthesis
- Product Name:4,4'-DIMETHOXYBENZIL
- CAS Number:1226-42-2
- Molecular formula:C16H14O4
- Molecular Weight:270.28
120-44-5
130 suppliers
$10.00/1g
1226-42-2
174 suppliers
$14.00/5g
Yield:1226-42-2 98%
Reaction Conditions:
with selenium(IV) dioxide in dimethyl sulfoxide at 170; for 0.0166667 h;Microwave irradiation;
Steps:
4.2.2. Experimental Procedure for Ethanediones 12 [36]
General procedure: Selenium dioxide (1.5 mmol) was added into a solutionof ethanone derivatives 11 (1 mmol) in DMSO (1.5 mL) andirradiated in the microwave oven for 1 min at 170C. The hotmixture was filtered to remove the selenium metal and thefiltrate was purified by column chromatography in silica gelusing EtOAc/hexanes 7:3 as eluent.
References:
Sangi, Diego P.;Cominetti, Márcia R.;Becceneri, Amanda B.;Resende, Flavia A.;Varanda, Eliana A.;Montanari, Carlos A.;Paix?o, Marcio W.;Corrêa, Arlene G. [Medicinal Chemistry,2015,vol. 11,# 8,p. 736 - 746]
18362-51-1
77 suppliers
$49.00/2g
1226-42-2
174 suppliers
$14.00/5g
2132-62-9
73 suppliers
$74.00/100mg
1226-42-2
174 suppliers
$14.00/5g
100-07-2
395 suppliers
$35.00/25g
1226-42-2
174 suppliers
$14.00/5g
119-52-8
139 suppliers
$8.00/5g
1226-42-2
174 suppliers
$14.00/5g