![453-20-3](/CAS/GIF/453-20-3.gif)
3-Hydroxytetrahydrofuran synthesis
- Product Name:3-Hydroxytetrahydrofuran
- CAS Number:453-20-3
- Molecular formula:C4H8O2
- Molecular Weight:88.11
![1,2,4-Butanetriol](/CAS/GIF/3068-00-6.gif)
3068-00-6
274 suppliers
$10.00/5g
![3-Hydroxytetrahydrofuran](/CAS/GIF/453-20-3.gif)
453-20-3
285 suppliers
$9.00/1g
Yield:453-20-3 96%
Reaction Conditions:
strong acid ion exchange resin (Amberlyst 15, H+ form) in 1,4-dioxane at 100; under 760.051 Torr; for 20 h;Product distribution / selectivity;
Steps:
1
Example 1; Instead of PEG-400 and the para-toluenesulfonic acid catalyst used in ComparativeExample 1, dioxane and a strong acid ion exchange resin (Amberlyst 15, H+ form) containing a sulfonic acid group were used in equal amounts. Then, the reaction was conducted using a batch type reactor under conditions of atmospheric pressure and 1000C for 20 hours. The reaction yield was 96 mol%.
References:
WO2007/81065,2007,A1 Location in patent:Page/Page column 6
![3-Buten-1-ol](/CAS/GIF/627-27-0.gif)
627-27-0
404 suppliers
$8.00/1g
![3-Hydroxytetrahydrofuran](/CAS/GIF/453-20-3.gif)
453-20-3
285 suppliers
$9.00/1g
![3,4-Epoxytetrahydrofuran](/CAS/GIF/285-69-8.gif)
285-69-8
193 suppliers
$6.00/1g
![3-Hydroxytetrahydrofuran](/CAS/GIF/453-20-3.gif)
453-20-3
285 suppliers
$9.00/1g
![1,4-Anhydroerythritol](/CAS/GIF/4358-64-9.gif)
4358-64-9
101 suppliers
$27.00/1g
![3-Hydroxytetrahydrofuran](/CAS/GIF/453-20-3.gif)
453-20-3
285 suppliers
$9.00/1g
![Dimethyl malate](/CAS/GIF/38115-87-6.gif)
38115-87-6
56 suppliers
inquiry
![3-Hydroxytetrahydrofuran](/CAS/GIF/453-20-3.gif)
453-20-3
285 suppliers
$9.00/1g
![Trimethyl borate](/CAS/GIF/121-43-7.gif)
121-43-7
359 suppliers
$14.00/25mL
![1,2,4-Butanetriol](/CAS/GIF/3068-00-6.gif)
3068-00-6
274 suppliers
$10.00/5g