3-Hydroxytetrahydrofuran synthesis
- Product Name:3-Hydroxytetrahydrofuran
- CAS Number:453-20-3
- Molecular formula:C4H8O2
- Molecular Weight:88.11
3068-00-6
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$10.00/5g
453-20-3
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$9.00/1g
Yield:453-20-3 96%
Reaction Conditions:
strong acid ion exchange resin (Amberlyst 15, H+ form) in 1,4-dioxane at 100; under 760.051 Torr; for 20 h;Product distribution / selectivity;
Steps:
1
Example 1; Instead of PEG-400 and the para-toluenesulfonic acid catalyst used in ComparativeExample 1, dioxane and a strong acid ion exchange resin (Amberlyst 15, H+ form) containing a sulfonic acid group were used in equal amounts. Then, the reaction was conducted using a batch type reactor under conditions of atmospheric pressure and 1000C for 20 hours. The reaction yield was 96 mol%.
References:
WO2007/81065,2007,A1 Location in patent:Page/Page column 6
627-27-0
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453-20-3
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453-20-3
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4358-64-9
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453-20-3
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453-20-3
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$9.00/1g
121-43-7
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3068-00-6
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$10.00/5g