3-[2-(1-PIPERIDINYL)ETHYL]INDOLE synthesis
- Product Name:3-[2-(1-PIPERIDINYL)ETHYL]INDOLE
- CAS Number:26628-87-5
- Molecular formula:C15H20N2
- Molecular Weight:228.33
14446-67-4
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201230-82-2
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100-63-0
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Yield:26628-87-5 97%
Reaction Conditions:
Stage #1: N-allylpiperidine;carbon monoxide;phenylhydrazinewith hydrogen;4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;Rh(acac)2(CO)2 in tetrahydrofuran at 70; under 15001.2 Torr; for 72 h;
Stage #2: with sulfuric acid for 2 h;Heating;
References:
Schmidt, Axel M.;Eilbracht, Peter [Journal of Organic Chemistry,2005,vol. 70,# 14,p. 5528 - 5535]
110-89-4
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