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ChemicalBook CAS DataBase List 2-(TERT-BUTOXYCARBONYLAMINO)PYRIDINE
38427-94-0

2-(TERT-BUTOXYCARBONYLAMINO)PYRIDINE synthesis

9synthesis methods
36016-38-3 Synthesis
tert-Butyl N-hydroxycarbamate

36016-38-3
350 suppliers
$6.00/5g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: triethylamine / tetrahydrofuran / 0.67 h / -20 °C
2.1: N,O-bis-(trimethylsilyl)-acetamide / 1,4-dioxane / 3 h / 80 °C
2.2: 3 h / 20 °C

References:

Fier, Patrick S.;Kim, Suhong;Cohen, Ryan D. [Journal of the American Chemical Society,2020,vol. 142,# 19,p. 8614 - 8618]

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