2,6-Dimethyl-4H-pyran-4-one synthesis
- Product Name:2,6-Dimethyl-4H-pyran-4-one
- CAS Number:1004-36-0
- Molecular formula:C7H8O2
- Molecular Weight:124.14
10556-93-1
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1004-36-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) lithium bis(trimethylsilyl)amide / 1.) THF, -78 deg C, 30 min, 2.) gradually warmed to room temp., 2-3 h, room temp.
2: 65 percent / trifluoroacetic acid / benzene / Ambient temperature; 12-18 h
References:
Koreeda, Masato;Akagi, Hiroshi [Tetrahedron Letters,1980,vol. 21,p. 1197 - 1200]
5456-14-4
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1004-36-0
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19396-77-1
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520-45-6
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1004-36-0
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771-03-9
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1004-36-0
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