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ChemicalBook CAS DataBase List 2,6-DI(CHLOROMETHYL)PYRIDINE HCL
94001-65-7

2,6-DI(CHLOROMETHYL)PYRIDINE HCL synthesis

11synthesis methods
-

Yield:94001-65-7 93%

Reaction Conditions:

Stage #1: 1-bromo-4-methoxy-benzenewith magnesium in diethyl ether;Grignard reaction;
Stage #2: acetophenone in diethyl ether; for 2 h;Heating;Further stages.;

References:

Van Walree, Cornelis A.;Kaats-Richters, Veronica E. M.;Veen, Sandra J.;Wieczorek, Birgit;Van Der Wiel, Johanna H.;Van Der Wiel, Bas C. [European Journal of Organic Chemistry,2004,# 14,p. 3046 - 3056]

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