2,3-Dihydro-2,2-dimethyl-7-benzofuranol synthesis
- Product Name:2,3-Dihydro-2,2-dimethyl-7-benzofuranol
- CAS Number:1563-38-8
- Molecular formula:C10H12O2
- Molecular Weight:164.2
120-80-9
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563-47-3
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1563-38-8
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$14.00/5g
Yield:1563-38-8 76.2%
Reaction Conditions:
in toluene at 144.84; for 4 h;Autoclave;Reagent/catalyst;Temperature;Time;
Steps:
Synthesis of benzofuranol
3.0 mmol of pyrocatechol, calculated amounts of3-chloro-2-methylpropene and ILs were added to a 100 mL Parr reactor with 23 mL of toluene. The reaction mixture was heated to 418 K and held constant for the desired time. The resultant mixture formed two layers after cooling to ambient temperature, and theupper phase was separated and analysed using a capillary GC (SGE BPX5: 30 m × 0.25 mm × 0.25 m)equipped with a flame ionisation detector and o-xyleneas an internal standard. The toluene in the separated upper phase was removed by distillation and the yieldof benzofuranol was obtained.
References:
Zhou, Han-Cheng;Li, Xiu-Lei;Liu, Juan-Li;Peng, Cheng;Zhang, Bin;Chen, Jin;Su, Qiong;Wu, Lan;Yuan, You-Zhu [Chemical Papers,2015,vol. 69,# 10,p. 1361 - 1366]
![2-[(2-METHYL-2-PROPENYL)OXY]-PHENOL](/CAS/GIF/4790-71-0.gif)
4790-71-0
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1563-38-8
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1563-66-2
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1563-38-8
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104-15-4
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53889-58-0
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1563-38-8
181 suppliers
$14.00/5g
120-80-9
502 suppliers
$13.00/25g
563-47-3
251 suppliers
$10.00/5g
1563-38-8
181 suppliers
$14.00/5g
1310466-22-8
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