1-(3-Bromophenyl)piperazine synthesis
- Product Name:1-(3-Bromophenyl)piperazine
- CAS Number:31197-30-5
- Molecular formula:C10H13BrN2
- Molecular Weight:241.13
821-48-7
554 suppliers
$6.00/25g
591-19-5
324 suppliers
$10.00/10g
31197-30-5
126 suppliers
$20.00/250mg
Yield:31197-30-5 72%
Reaction Conditions:
Stage #1: bis-(2-chloroethyl)amine hydrochloride;m-Bromoaniline in butan-1-ol; for 48 h;Heating;
Stage #2: with sodium carbonate in butan-1-ol; for 24 h;Heating;
References:
Naito, Hiroyuki;Ohsuki, Satoru;Sugimori, Masamichi;Atsumi, Ryo;Minami, Megumi;Nakamura, Yoshihide;Ishii, Mineko;Hirotani, Kenji;Kumazawa, Eiji;Ejima, Akio [Chemical and pharmaceutical bulletin,2002,vol. 50,# 4,p. 453 - 462]