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1-Boc-3-piperidone

1-Boc-3-piperidone Struktur
98977-36-7
CAS-Nr.
98977-36-7
Englisch Name:
1-Boc-3-piperidone
Synonyma:
TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE;N-BOC-3-PIPERIDINONE;N-Boc-3-piperidone;1-BOC-piperidone;1-BOC-3-PIPERIDINONE;1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE;3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-Boc-3-Pipe;3-Oxopiperidine;BOC-3-PIPERIDONE
CBNumber:
CB8428473
Summenformel:
C10H17NO3
Molgewicht:
199.25
MOL-Datei:
98977-36-7.mol

1-Boc-3-piperidone Eigenschaften

Schmelzpunkt:
35-40 °C (lit.)
Siedepunkt:
289.8±33.0 °C(Predicted)
Dichte
1.099±0.06 g/cm3(Predicted)
Flammpunkt:
>230 °F
storage temp. 
2-8°C
pka
-1.71±0.20(Predicted)
Aggregatzustand
Liquid
Farbe
Clear colorless
Wasserl?slichkeit
It is insoluble in water.
BRN 
5936353
InChI
InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
InChIKey
RIFXIGDBUBXKEI-UHFFFAOYSA-N
SMILES
N1(C(OC(C)(C)C)=O)CCCC(=O)C1
CAS Datenbank
98977-36-7(CAS DataBase Reference)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
S-S?tze: 24/25
WGK Germany  3
HazardClass  KEEP COLD
HS Code  29339900
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
Sicherheit
P264 Nach Gebrauch gründlich waschen.
P264 Nach Gebrauch gründlich waschen.
P280 Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

1-Boc-3-piperidone Chemische Eigenschaften,Einsatz,Produktion Methoden

S-S?tze Betriebsanweisung:

S24/25:Berührung mit den Augen und der Haut vermeiden.

Chemische Eigenschaften

White to yellow low melting solid

Verwenden

1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.

Synthese

With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.

1-Boc-3-piperidone Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

(S)-3-Amino-1-N-Boc-piperidine 3-HYDROXY-3-PHENYL-PIPERIDINE 6-METHOXY-1,2,3,4-TETRAHYDRO-BETA-CARBOLINE 4,5,6,7-tetrahydro-1-methyl-1H-Pyrazolo[3,4-c]pyridine Aceton tert-butyl 3-(isopropylamino)piperidine-1-carboxylate 5-(Toluene-4-sulfonyloxy)-3,4-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester TERT-BUTYL 3-(N-BENZYL-N-METHYLAMINO) PIPERIDINE-1-CARBOXYLATE 1-N-BOC-3-HYDROXY-3-PHENYLPIPERIDINE

1-Boc-3-piperidone Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 501)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Chongqing Ensky Pharmaceutical Co.,Ltd.
+86-23-86815286 +86-13983794297
 sales@ensky-chemical.com China 92 58
Shanghai Quedan biology science and technology co., ltd
+86-13004146052
 lnzc@quedan.com.cn China 1022 58
Anhui Yisheng Technology Co., LTD
+86-19355901310 +86-19355901310
 alice@ah-yisheng.com China 319 58
Zhengzhou Lingzhiyue Technology Co., Ltd
+86-0371-55074660 +86-13783527580
 Lingzhiyue@aliyun.com China 3145 58
Anhui Yiao New Material Technology Co., Ltd 		+86-18033737140 +86-17354101231
 sales1@hbganmiao.com China 227 58
Xiamen Wonderful Bio Technology Co., Ltd. 		+8613043004613
 Sara@xmwonderfulbio.com China 283 58
Shandong Huisheng Import & Export Co., Ltd. 		+86-13176845580 +86-13176845580
 da@zhongda-biotech.com China 232 58
Anhui Zhongda Biotechnology Co., Ltd 		+8619956560829
 justine@zhongda-biotech.com China 286 58
Anhui Zhongda Biotechnology Co., Ltd 		+8615689548120
 linda@zhongda-biotech.com China 193 58
Anhui Ruihan Technology Co., Ltd 		+8617756083858
 daisy@anhuiruihan.com China 973 58

98977-36-7()Verwandte Suche:

  • T-BUTYL-3-PIPERIDONE-1-CARBOXYLATE
  • 3-OXOPIPERIDINE, N-BOC PROTECTED
  • 1-PIPERIDINECARBOXYLIC ACID, 3-OXO-, 1,1-DIMETHYLETHYL ESTER
  • 1-N-BOC-3-PIPERIDONE
  • 1-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
  • 1-BOC-3-PIPERIDONE
  • 1-BOC-PIPERIDIN-3-ONE
  • BOC-3-PIPERIDONE
  • N-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
  • 3-ketopiperidine-1-carboxylic acid tert-butyl ester
  • 3-oxo-1-piperidinecarboxylic acid tert-butyl ester
  • 1-(tert-Butoxycarbonyl)-3-piperidone
  • 1,1-Dimethylethyl 3-Oxo-1-Piperidine Carboxylate
  • Tert-butyl-3-oxo-1-piperidinecarboxylate
  • 1-Boc-3-piperidone,97%
  • 1-N-TERT-BUTOXYCARBONYL-3-PIPERIDONE
  • 3-Oxopiperidine, N-BOC protected 97%
  • 1-N-Boc-piperdine-3-one
  • N-BOC-3-piperidone,97%
  • 1-N-Boc-3-Piperidine
  • Piperidin-3-one, N-BOC protected 97%
  • tert-Butyl 3-oxopiperidine-1-carboxylate, 3-Oxopiperidine, N-BOC protected
  • N-(tert-Butoxycarbonyl)-3-piperidone
  • 1-Boc-3-piperidone 97%
  • N - bok - 3 - piperidine ketone
  • 1-Boc-3-piperidone tert-Butyl 3-oxopiperidine-1-carboxylate
  • 3-Oxopiperidine
  • Piperidin-3-one, N-BOC protected
  • 1-Boc-3-piperidone 98977-36-7
  • 98977-36-7 tert-Butyl 3-oxopiperidine-1-carboxylate
  • 1-BOC-3-oxopiperidine
  • 1-(tert-Butoxycarbonyl)-3-piperidone >
  • Ibrutinib Impurity 58
  • TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE
  • N-Boc-3-piperidone
  • N-BOC-3-PIPERIDINONE
  • 3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
  • 1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE
  • 1-BOC-3-PIPERIDINONE
  • 1-BOC-piperidone
  • 3-Oxo-piperidin-1-carboxylic acid tert-butyl ester
  • 1-Boc-3-Pipe
  • 98977-36-7
  • 99175-10-5
  • 9877-36-7
  • 989777-36-7
  • Building Blocks
  • Piperidones
  • Heterocyclic Building Blocks
  • Piperidines
  • Pharmaceutical Intermediates
  • pharmacetical
  • Pyrans, Piperidines &Piperazines
  • Acids and Derivatives
  • Carbonyl Compounds
  • Pyrans, Piperidines & Piperazines
  • Building Blocks
  • Heterocyclic Building Blocks
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