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Tricyclo[3.3.1.13,7]decan-1-ol

1-Adamantanol Struktur
768-95-6
CAS-Nr.
768-95-6
Bezeichnung:
Tricyclo[3.3.1.13,7]decan-1-ol
Englisch Name:
1-Adamantanol
Synonyma:
ADAMANTANOL;ADAMANTAN-1-OL;1-Adamantol;1-Admantanol;(3s,5s,7s)-adamantan-1-ol;1-AD-OH;1-HYDROXYADAMANTANE;1-ADA-OH;AKOS BC-0650;damantol-(1)
CBNumber:
CB2135047
Summenformel:
C10H16O
Molgewicht:
152.23
MOL-Datei:
768-95-6.mol

Tricyclo[3.3.1.13,7]decan-1-ol Eigenschaften

Schmelzpunkt:
247 °C (subl.) (lit.)
Siedepunkt:
214.73°C (rough estimate)
Dichte
0.8544 (rough estimate)
Brechungsindex
1.4880 (estimate)
Flammpunkt:
240°C
storage temp. 
Sealed in dry,Room Temperature
L?slichkeit
Chloroform (Sparingly), Methanol (Slightly)
pka
15.38±0.20(Predicted)
Aggregatzustand
Crystalline Powder or Needles
Farbe
White to off-white
Wasserl?slichkeit
Soluble in ethanol , methanol, and diethyl ether. Partly miscible in water.
Sublimation 
240 ºC
BRN 
1903952
InChIKey
VLLNJDMHDJRNFK-UHFFFAOYSA-N
CAS Datenbank
768-95-6(CAS DataBase Reference)
NIST chemische Informationen
1-Adamantanol(768-95-6)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher Xi
R-S?tze: 36/37/38
S-S?tze: 22-24/25-36-26
WGK Germany  3
RTECS-Nr. AU4980000
Hazard Note  Irritant
HS Code  29061900
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizit?t (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" />
Sicherheit
P261 Einatmen von Staub vermeiden.
P271 Nur im Freien oder in gut belüfteten R?umen verwenden.
P280 Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.

Tricyclo[3.3.1.13,7]decan-1-ol Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.

S-S?tze Betriebsanweisung:

S22:Staub nicht einatmen.
S24/25:Berührung mit den Augen und der Haut vermeiden.
S36:DE: Bei der Arbeit geeignete Schutzkleidung tragen.
S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.

Beschreibung

1-Adamantanol is a cyclic molecule with a hydroxyl group. It is produced by the oxidation of 2-methyl-2-adamantanol. 1-Adamantanol has been shown to be an effective substrate for bioremediation in wastewater treatment plants and can be used as a precursor to produce trifluoroacetic acid.

Chemische Eigenschaften

white to off-white crystalline powder or needles

Verwenden

1-Adamantanol was used in the preparation of 1,3-adamantanediol. It is used in the manufacture of synthetic adamantane derivatives and adapalene.

l?uterung methode

If 2-adamantanol is a suspected impurity, then dissolve the substance (10g) in acetone (100mL) and add Jones's reagent [CrO3 (10.3g) in H2O (30mL)], then conc H2SO4 (8.7mL) is added dropwise (turns green in colour) until excess reagent is present (slight red colour). Stir overnight, decant the acetone solution from the Cr salts and adamantan-2-one, dry (Na2SO4) and evaporate to dryness. The residue (ca 7g) is chromatographed through Al2O3 (250g) and washed with 50% *benzene/pet ether (b 40-60o), then 100% Et2O (to remove any adamantan-2-one present) and the 1-adamantanol is then eluted with 5% MeOH in Et2O. The eluate is evaporated, and the residue is recrystallised from pet ether (b 30-60o) at -70o, m 287.2-288.5o. It also crystallises from MeOH and can be sublimed in vacuo. It has characteristic IR, max 3640, 1114, 1086, 982 and 930cm-1. [Schleyer & Nicholas J Am Chem Soc 83 182 1961.] [Beilstein 6 IV 391.] Alternatively, if free from the 2-isomer, dissolve it in tetrahydrofuran, dilute with H2O to precipitate the alcohol. Collect, dry and sublime it in a vacuum at 130o. [Stetter et al. Chem Ber 92 1629 1959.]

Tricyclo[3.3.1.13,7]decan-1-ol Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Tricyclo[3.3.1.13,7]decan-1-ol Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

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768-95-6(Tricyclo[3.3.1.13,7]decan-1-ol)Verwandte Suche:


  • TRICYCLO[3.3.1.1(3,7)]DECAN-1-OL
  • TRICYCLO[3.3.1.1]DECAN-1-OL
  • 1-HYDROXYDIAMANTANE
  • 1-ADA-OH
  • 1-ADAMANTANOL
  • 1-Adamatanol
  • -Adamantyl alcohol
  • damantol-(1)
  • tricyclo(3.3.1.1(sup3,7))decan-1-ol
  • ADAMANTANOL, 1-
  • AKOS BC-0650
  • 1-Adamantonal
  • 1-Adamantanol,98%
  • LABOTEST-BB LT00436924
  • ADAMANTANOL, 1-(SG)
  • (1-Adamantyl) alcohol
  • Adamantan-3-ol
  • Hydroxyadamantane
  • 1-Adamantanol,99%
  • Tricyclo[3,3,1,1]3,7 decanol-1
  • adamantan-1-ol(SALTDATA: FREE)
  • 1-AdaMantanol, 99% 5GR
  • 1-ADAMANTANOL FOR SYNTHESIS 10 G
  • Adapalene IMpurity H
  • Adamantan-1-ol, Tricyclo[3.3.1.1~3,7~]decan-1-ol
  • 1-Adamantanol Vetec(TM) reagent grade, 98%
  • Tricyclo(3.3.1.1(sup 3,7))decan-1-ol (9CI)
  • 1-AdaMantanol ReagentPlus(R), 99%
  • 1 - adaMantane alcohol
  • 1-Adamanthanol/Adamantan-1-ol
  • 1-Adamantano
  • 1 Adamentanol (768-95-6)
  • 1-Adamantanol >
  • 1-HYDROXYADAMANTANE
  • 1-AD-OH
  • 1-Adamantol
  • ADAMANTANOL
  • ADAMANTAN-1-OL
  • 1-Admantanol
  • (3s,5s,7s)-adamantan-1-ol
  • 1-Adamantanol (6CI, 7CI, 8CI)
  • 1-HYDROXY ADAMANTANE (1-adamantanol)
  • HYDROXY ADAMANTANE (1-ADAMANTANOL)
  • 768-95-6
  • C9 to C30
  • Alcohols
  • Building Blocks
  • Oxygen Compounds
  • Organic Building Blocks
  • Adamantanes
  • Alcohols
  • Building Blocks
  • C9 to C10
  • Chemical Synthesis
  • Organic Building Blocks
  • Oxygen Compounds
  • FINE Chemical & INTERMEDIATES
  • Adamantane derivatives
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