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ChemicalBook--->CAS DataBase List--->91-52-1

91-52-1

91-52-1 Structure

91-52-1 Structure
IdentificationMore
[Name]

2,4-Dimethoxybenzoic acid
[CAS]

91-52-1
[Synonyms]

2,4-DIMETHOXYBENZOIC ACID
B-RESORCYLIC ACID DIMETHYL ETHER
DIMETHOXYBENZOIC-2,4 ACID
DIMETHOXYBENZOIC ACID,2,4-
RARECHEM AL BO 0028
2,4-dimethoxy-benzoicaci
2,4-Dimethoxybenzoic acid, 98+%
2,4-Dimethoxybenzoic
Benzoic acid, 2,4-dimethoxy-
DIMETHOXYBENZOIC ACID,2,4-(RG)
[EINECS(EC#)]

202-074-1
[Molecular Formula]

C9H10O4
[MDL Number]

MFCD00002434
[Molecular Weight]

182.17
[MOL File]

91-52-1.mol
Chemical PropertiesBack Directory
[Appearance]

white to off-white powder
[Melting point ]

107-109 °C (lit.)
[Boiling point ]

275.56°C (rough estimate)
[density ]

1.2481 (rough estimate)
[refractive index ]

1.4500 (estimate)
[storage temp. ]

Sealed in dry,Room Temperature
[form ]

Powder
[pka]

4.36±0.10(Predicted)
[color ]

White to off-white
[Water Solubility ]

slightly soluble
[BRN ]

2210860
[InChIKey]

GPVDHNVGGIAOQT-UHFFFAOYSA-N
[LogP]

1.588 (est)
[CAS DataBase Reference]

91-52-1(CAS DataBase Reference)
[NIST Chemistry Reference]

Benzoic acid, 2,4-dimethoxy-(91-52-1)
[EPA Substance Registry System]

91-52-1(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37/39:Wear suitable gloves and eye/face protection .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[TSCA ]

Yes
[HS Code ]

29189090
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Sodium hydroxide-->Hydrochloric acid-->Dimethyl sulfate-->2,4-Dihydroxybenzoic acid-->Benzene, 1-ethenyl-2,4-dimethoxy--->2,4-diacetyloxybenzoic acid-->BIS(ALPHA-CHLOROETHYL)ETHER-->1-Bromo-2,4-dimethoxybenzene-->2,4-DIMETHOXYBENZALDOXIME-->4-Methoxysalicylic acid
[Preparation Products]

METHYL 2,4-DIMETHOXYBENZOATE-->2,4-Dimethoxyphenylacetic acid-->2,4-Dimethoxybenzyl alcohol-->N,2,4-trimethoxy-N-methylbenzamide
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

2,4-Dimethoxybenzoic acid(91-52-1).msds
Hazard InformationBack Directory
[Chemical Properties]

white to off-white powder
[Uses]

Yttrium and heavy lanthanide complexes is synthesised with 2, 4-dimethoxybenzoic acid and thermal and spectral features is studied. In the case of the electron-rich aromatic system 2,4-dimethoxybenzoic acid reduction of the intermediate HOBt ester is slow, and good.
[Purification Methods]

Crystallise the acid from water and dry it in a vacuum desiccator over H2SO4.. The S-benzylisothiuronium salt has m 158-159o (from CHCl3). [Beilstein 10 H 379, 10 I 177, 10 II 252, 10 III 1371, 10 IV 1422.] Aromatic acid impurities (to <0.05%) can be removed via the (±)--methylbenzylamine salt as described for 2,4-dichlorobenzoic acid [Ley & Yates Organic Process Research & Development 12 120 2008.]
Spectrum DetailBack Directory
[Spectrum Detail]

2,4-Dimethoxybenzoic acid(91-52-1)MS
2,4-Dimethoxybenzoic acid(91-52-1)1HNMR
2,4-Dimethoxybenzoic acid(91-52-1)IR1
2,4-Dimethoxybenzoic acid(91-52-1)IR2
2,4-Dimethoxybenzoic acid(91-52-1)Raman
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

2,4-Dimethoxybenzoic acid, 98%(91-52-1)
[Sigma Aldrich]

91-52-1(sigmaaldrich)
[TCI AMERICA]

2,4-Dimethoxybenzoic Acid,>99.0%(T)(91-52-1)
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