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ChemicalBook--->CAS DataBase List--->586-77-6

586-77-6

586-77-6 Structure

586-77-6 Structure
IdentificationMore
[Name]

4-Bromo-N,N-dimethylaniline
[CAS]

586-77-6
[Synonyms]

4-BROMO-N,N-DIMETHYLANILINE
N-(4-BROMOPHENYL)-N,N-DIMETHYLAMINE
N,N-DIMETHYL-P-BROMOANILINE
P-BROMO-N,N-DIMETHYLANILINE
(4-Bromo-phenyl)-dimethyl-amine
1-Bromo-4-(dimethylamino)benzene
4-(Dimethylamino)phenyl bromide
4-(dimethylamino)phenylbromide
4-bromo-dimethylaniline
4-bromo-n,n-dimethyl-anilin
4-bromo-n,n-dimethyl-benzenamin
4-Bromo-N,N-dimethylbenzenamine
4-bromo-N,N-dimethyl-Benzenamine
4-Dimethylaminobromobenzene
Aniline, 4-bromo-N,N-dimethyl-
Aniline, p-bromo-N,N-dimethyl-
Benzenamine, 4-bromo-N,N-dimethyl-
N,N-Dimethyl-4-bromoaniline
p-(Dimethylamino)phenyl bromide
p-(dimethylamino)phenylbromide
[EINECS(EC#)]

209-582-2
[Molecular Formula]

C8H10BrN
[MDL Number]

MFCD00000093
[Molecular Weight]

200.08
[MOL File]

586-77-6.mol
Chemical PropertiesBack Directory
[Appearance]

white to light grey powder
[Melting point ]

52-54 °C (lit.)
[Boiling point ]

264 °C (lit.)
[density ]

1.3220
[refractive index ]

1.5748 (estimate)
[Fp ]

>230 °F
[storage temp. ]

2-8°C
[solubility ]

Chloroform, Methanol
[form ]

Crystalline Solid
[pka]

4.23(at 25℃)
[color ]

White to gray or light blue
[Stability:]

Stable. Incompatible with oxidizing agents, acids, metals.
[Water Solubility ]

Soluble in methanol. Insoluble in water.
[BRN ]

2206155
[InChIKey]

XYZWMVYYUIMRIZ-UHFFFAOYSA-N
[CAS DataBase Reference]

586-77-6(CAS DataBase Reference)
[NIST Chemistry Reference]

4-Bromo-N,N-dimethylaniline(586-77-6)
[EPA Substance Registry System]

586-77-6(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
R36/38:Irritating to eyes and skin .
R33:Danger of cumulative effects.
R22:Harmful if swallowed.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S37:Wear suitable gloves .
[RIDADR ]

2811
[WGK Germany ]

3
[RTECS ]

BW9300000
[F ]

8
[Hazard Note ]

Irritant
[TSCA ]

Yes
[HazardClass ]

6.1(b)
[PackingGroup ]

III
[HS Code ]

29214290
Raw materials And Preparation ProductsBack Directory
[Raw materials]

N,N-Dimethylaniline
[Preparation Products]

4-(Dimethylamino)phenylboronic acid-->methoxymethanol-->4,4'-VINYLIDENEBIS(N,N-DIMETHYLANILINE)-->4-Iodo-N,N-dimethyl-Benzenamine-->p-(Dimethylamino)benzenesulfonyl chloride-->4'-DIMETHYLAMINOPHENYL ACETYLENE-->4-(DIMETHYLAMINO)BENZONITRILE-->CYTXUPXHVXSDML-UHFFFAOYSA-N
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

4-Bromo-N,N-dimethylaniline(586-77-6).msds
Hazard InformationBack Directory
[Chemical Properties]

white to light grey powder
[Uses]

4-Bromo-N,N-dimethylaniline is used as an internal standard in the determination of iodine present as iodide (as in pharmaceuticals), iodate (as in iodized table salt) and covalently bound to organic compounds (as in milk and vegetables).
[Purification Methods]

Reflux the aniline for 3hours with two equivalents of acetic anhydride, then fractionally distil it under reduced pressure. [Beilstein 12 IV 1499.]
Spectrum DetailBack Directory
[Spectrum Detail]

4-Bromo-N,N-dimethylaniline(586-77-6)MS
4-Bromo-N,N-dimethylaniline(586-77-6)1HNMR
4-Bromo-N,N-dimethylaniline(586-77-6)13CNMR
4-Bromo-N,N-dimethylaniline(586-77-6)IR1
4-Bromo-N,N-dimethylaniline(586-77-6)IR2
4-Bromo-N,N-dimethylaniline(586-77-6)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

4-Bromo-N,N-dimethylaniline, 99%(586-77-6)
[Alfa Aesar]

4-Bromo-N,N-dimethylaniline, 98+%(586-77-6)
[Sigma Aldrich]

586-77-6(sigmaaldrich)
[TCI AMERICA]

4-Bromo-N,N-dimethylaniline,>97.0%(GC)(586-77-6)
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