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ChemicalBook--->CAS DataBase List--->20277-69-4

20277-69-4

20277-69-4 Structure

20277-69-4 Structure
IdentificationMore
[Name]

Sodium methanesulphinate
[CAS]

20277-69-4
[Synonyms]

METHANESULFINIC ACID
METHANESULFINIC ACID SODIUM SALT
METHANESULPHINIC ACID SODIUM SALT
SODIUM METHANESULFINATE
sodium methanesulphinate
SODIUM METHANESULFINATE, TECH., 85%
Methanesulfinic acid sodium salt, tech. 85%
[EINECS(EC#)]

243-669-6
[Molecular Formula]

CH3NaO2S
[MDL Number]

MFCD00040392
[Molecular Weight]

102.09
[MOL File]

20277-69-4.mol
Chemical PropertiesBack Directory
[Appearance]

White to light beige powder
[Melting point ]

222-226 °C (dec.) (lit.)
[storage temp. ]

Inert atmosphere,Room Temperature
[solubility ]

Methanol, Water (Slightly)
[form ]

Powder
[color ]

White to light beige
[Water Solubility ]

soluble
[Sensitive ]

Air Sensitive & Hygroscopic
[BRN ]

3565430
[Stability:]

Hygroscopic
[InChI]

InChI=1S/CH4O2S.Na.H/c1-4(2)3;;/h1H3,(H,2,3);;
[InChIKey]

LYPGDCWPTHTUDO-UHFFFAOYSA-M
[SMILES]

S(O)(=O)C.[NaH]
[CAS DataBase Reference]

20277-69-4(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn
[Risk Statements ]

R22:Harmful if swallowed.
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S36/37:Wear suitable protective clothing and gloves .
[RIDADR ]

2811
[WGK Germany ]

3
[PackingGroup ]

III
[HS Code ]

29309090
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Methanesulfinylchloride-->Methanesulfonyl iodide (7CI,9CI)-->Methanesulfonamide, N-hydroxy-N-(methylsulfonyl)--->2,3-dihydrothiophene 1,1-dioxide-->P-NITROSOTOLUENE-->3-SULFOLENE-->Sodium nitrite
[Preparation Products]

Disperse Orange 29-->SIRIUS YELLOW GC-->disodium 3,3'-[carbonylbis[imino(3-methoxy-4,1-phenylene)azo]]dibenzoate-->synthetic tanning agent No.28-->2-Fluoro-4-(methylsulfonyl)aniline-->Zonisamide-->4-Bromo-2-fluoro-1-(methylsulfonyl)benzene-->METHYLSULFONYLACETONE-->4-(METHYLSULFONYL)BENZONITRILE-->Methyl 6-(methylsulfonyl)nicotinate
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

Methanesulfinic acid sodium salt(20277-69-4).msds
Questions And AnswerBack Directory
[Description]

Sodium methanesulfinate is an aliphatic sodium sulfinate. Conjugate addition of sodium methanesulfinate to vinyl heterocycles has been described. Cross-coupling reaction between aryl boronic acid and sodium methanesulfinate has been studied. It can be used in the preparation of alkyl methyl sulfone and methyl bis(4-tolyl)sulfoniumtrifluoromethanesulfonate. It is also employed in the synthesis of two sulfonyl type reversible addition-fragmentation transfer (RAFT) agents such as benzyl methylsulfonyldithioformate and benzyl phenylsulfonyldithioformate. Moreover, it can be used for synthesizing cyclooxygenase-2 inhibitors.
Hazard InformationBack Directory
[Chemical Properties]

White to light beige powder
[Uses]

Sodium methylsulfinate can be used to synthesize cyclooxygenase-2 inhibitors.
[General Description]

Sodium methanesulfinate is an aliphatic sodium sulfinate. Conjugate addition of sodium methanesulfinate to vinyl heterocycles has been described. Cross-coupling reaction between aryl boronic acid and sodium methanesulfinate has been studied. Its stock solution was prepared from methanesulfonic acid by adding one equivalent of sodium hydroxide and diluting it to 4M.
Spectrum DetailBack Directory
[Spectrum Detail]

Sodium methanesulfinate(20277-69-4)1HNMR
Sodium methanesulfinate(20277-69-4)13CNMR
Sodium methanesulfinate(20277-69-4)IR1
Sodium methanesulfinate(20277-69-4)IR2
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

Methanesulfinic acid, sodium salt, 85%(20277-69-4)
[Alfa Aesar]

Methanesulfinic acid sodium salt, 95%(20277-69-4)
[Sigma Aldrich]

20277-69-4(sigmaaldrich)
[TCI AMERICA]

Sodium Methanesulfinate,>90.0%(T)(20277-69-4)
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