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ChemicalBook--->CAS DataBase List--->108-69-0

108-69-0

108-69-0 Structure

108-69-0 Structure
IdentificationMore
[Name]

3,5-Dimethylaniline
[CAS]

108-69-0
[Synonyms]

1-AMINO-3,5-DIMETHYLBENZENE
3,5-DIMETHYLANILINE
3,5-XYLIDINE
5-AMINO-M-XYLENE
AKOS BBS-00003574
1-amino-3,5-dimethyl-benzen
3,5-dimethyl-benzenamin
3,5-Dimethylbenzenamine
3,5-dimethyl-Benzenamine
3,5-Dimethylbenzeneamine
3,5-Dimethylphenylamine
3,5-Xylidene
3,5-Xylylamine
5-Amino-1,3-dimethylbenzene
5-Amino-1,3-xylene
3,5-Diemthylaniline
3,5-DIMETHYLANILINE (3,5-XYLIDENE)
3,5-Dimethy Iani line
3,5-DIMETHYLANILINE(3,5-XYLIDINE)
3,5-DIMETHYLBENZAMINE
[EINECS(EC#)]

203-607-0
[Molecular Formula]

C8H11N
[MDL Number]

MFCD00007813
[Molecular Weight]

121.18
[MOL File]

108-69-0.mol
Chemical PropertiesBack Directory
[Appearance]

clear yellow-brown to brown liquid
[Melting point ]

7-9 °C
[Boiling point ]

104-105 °C14 mm Hg(lit.)
[density ]

0.972 g/mL at 25 °C(lit.)
[vapor pressure ]

1.3-27hPa at 20-100℃
[refractive index ]

n20/D 1.557(lit.)
[Fp ]

200 °F
[form ]

Liquid
[pka]

pK1:4.765(+1) (25°C)
[color ]

Clear yellow-brown to brown
[Water Solubility ]

<0.1 g/100 mL at 19 ºC
[Merck ]

14,10084
[BRN ]

507051
[Concentration]

0.1 mCi/ml
[Solvent]

Ethanol
[Specific Activity]

50-60 mCi/mmol
[InChIKey]

MKARNSWMMBGSHX-UHFFFAOYSA-N
[Dissociation constant]

4.71-4.91 at 15-25℃
[CAS DataBase Reference]

108-69-0(CAS DataBase Reference)
[NIST Chemistry Reference]

Benzenamine, 3,5-dimethyl-(108-69-0)
[EPA Substance Registry System]

108-69-0(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

T,N
[Risk Statements ]

R23/24/25:Toxic by inhalation, in contact with skin and if swallowed .
R33:Danger of cumulative effects.
R51/53:Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment .
[Safety Statements ]

S28:After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer) .
S36/37:Wear suitable protective clothing and gloves .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S61:Avoid release to the environment. Refer to special instructions safety data sheet .
[RIDADR ]

UN 1711 6.1/PG 2
[WGK Germany ]

3
[RTECS ]

ZE9625000
[F ]

8
[Hazard Note ]

Toxic
[TSCA ]

Yes
[HazardClass ]

6.1
[PackingGroup ]

II
[HS Code ]

29214990
[Safety Profile]

Suspected carcinogen. Moderately toxic by ingestion. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also other xylidine entries.
[Hazardous Substances Data]

108-69-0(Hazardous Substances Data)
Raw materials And Preparation ProductsBack Directory
[Raw materials]

3,5-Dimethylphenol-->5-Bromo-m-xylene
[Preparation Products]

2-(TRIFLUOROMETHYL)-5,7-DIMETHYLQUINOLINE-4-CARBOXYLIC ACID-->3,5-DIMETHYLPHENYL ISOTHIOCYANATE-->1-Iodo-3,5-dimethylbenzene-->Efaproxiral-->2,5-DIBROMO-M-XYLENE-->3,5-Dimethylphenylhydrazine hydrochloride-->tetrasodium 5-(acetylamino)-3-[[4-[[3,5-dimethyl-4-[(8-sulphonato-2-naphthyl)azo]phenyl]azo]-2-ethoxy-6-sulphonato-1-naphthyl]azo]-4-hydroxynaphthalene-2,7-disulphonate-->1-(3,5-DIMETHYLPHENYL)-5-OXOPYRROLIDINE-3-CARBOXYLIC ACID-->2-BROMO-N-(3,5-DIMETHYL-PHENYL)-ACETAMIDE-->3-(3,5-DIMETHYL-PHENYLAMINO)-PROPIONITRILE
Hazard InformationBack Directory
[General Description]

Dark brown liquid.
[Reactivity Profile]

3,5-XYLIDINE(108-69-0) ignites on contact with fuming nitric acid . Neutralizes acids in exothermic reactions to form salts plus water. May be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. Flammable gaseous hydrogen may be generated in combination with strong reducing agents, such as hydrides.
[Air & Water Reactions]

This chemical may be sensitive to prolonged exposure to air. Insoluble in water.
[Fire Hazard]

This chemical is combustible.
[Chemical Properties]

clear yellow-brown to brown liquid
[Uses]

3,5-Dimethylaniline is the reagent commonly useful in the manufacture of dyes. It undergoes polymerization in the presence of cerium(IV) sulfate as an oxidant. 3,5-Dimethylaniline was used in the synthesis of chiral packing materials for high performance liquid chromatography.
[Purification Methods]

Convert sym-xylidine to a derivative (see below) which, after recrystallisation, is decomposed with alkali to give the free base. Dry it over KOH and fractionally distil it. The acetyl derivative has m 144o, the benzoyl derivative has m 136o and the picrate has m 209o (from H2O, EtOH or 10% AcOH). [Beilstein 12 H 1131, 12 IV 2561.]
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

5-Amino-m-xylene(108-69-0).msds
Spectrum DetailBack Directory
[Spectrum Detail]

3,5-Dimethylaniline(108-69-0)MS
3,5-Dimethylaniline(108-69-0)1HNMR
3,5-Dimethylaniline(108-69-0)13CNMR
3,5-Dimethylaniline(108-69-0)IR1
3,5-Dimethylaniline(108-69-0)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

3,5-Dimethylaniline, 98%(108-69-0)
[Alfa Aesar]

3,5-Dimethylaniline, 97+%(108-69-0)
[Sigma Aldrich]

108-69-0(sigmaaldrich)
[TCI AMERICA]

3,5-Dimethylaniline,>98.0%(GC)(108-69-0)
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