Zinc acetate synthesis
- Product Name:Zinc acetate
- CAS Number:557-34-6
- Molecular formula:C4H6O4Zn
- Molecular Weight:183.48
5970-45-6
348 suppliers
$13.50/25G
64-19-7
1553 suppliers
$10.00/25ML
557-34-6
537 suppliers
$21.00/5g
Yield:557-34-6 84%
Reaction Conditions:
Stage #1: acetic acidwith sodium hydrogencarbonate in methanol;water at 25; for 2 h;
Stage #2: zinc(II) acetate dihydrate in methanol;water at 50; for 2 h;
Steps:
2.3. Synthesis
Aqueous solution of sodium salt of cinnamic or acetic acid, obtained by reacting2 mmole of the respective acid with equimolar amount of sodium bicarbonate, was added dropwise into aqueous solution of zinc(II) acetate dihydrate in mole ratio 2:1.The reaction mixture was stirred for two hours at 50 C, the resultant solid productwas filtered, washed and air dried to get the precursors (I1 and I2). The precursor wasdissolved in methanol with subsequent addition of the respective secondary ligand toit. The reaction mixture was stirred again for another 3-4 h under ambient temperature.The clear solution, thus obtained, was left for evaporation at room temperatureto obtain 1-8.
References:
Zahoor, Ayesha;Imtiaz-Ud-Din;Andleeb, Sohaila;Raheel, Ahmad;Ayub, Rabia;Abbas, Sumaira;Tahir, Muhammad Nawaz [Journal of Coordination Chemistry,2021,vol. 74,# 12,p. 1978 - 1991]
5970-45-6
348 suppliers
$13.50/25G
557-34-6
537 suppliers
$21.00/5g
557-20-0
231 suppliers
$14.00/1g
557-34-6
537 suppliers
$21.00/5g
591-87-7
185 suppliers
$10.00/10g
28557-00-8
0 suppliers
inquiry
300-57-2
223 suppliers
$53.00/25mL
92-52-4
397 suppliers
$9.00/5g
557-34-6
537 suppliers
$21.00/5g
127-09-3
1068 suppliers
$8.00/100dtn(0.82g)
7440-66-6
11 suppliers
$14.00/5g
557-34-6
537 suppliers
$21.00/5g