TRIS(PENTAFLUOROPHENYL)PHOSPHINE synthesis
- Product Name:TRIS(PENTAFLUOROPHENYL)PHOSPHINE
- CAS Number:1259-35-4
- Molecular formula:C18F15P
- Molecular Weight:532.14
344-04-7
377 suppliers
$9.00/5g
1259-35-4
149 suppliers
$16.00/1g
Yield:1259-35-4 31%
Reaction Conditions:
Stage #1:bromopentafluorobenzene with magnesium in diethyl ether at -6.16;Inert atmosphere;
Stage #2: with phosphorus tribromide in diethyl ether at 20; for 1 h;Inert atmosphere;
References:
Schaefer, Andre;Reissmann, Matti;Schaefer, Annemarie;Saak, Wolfgang;Haase, Detlev;Mueller, Thomas [Angewandte Chemie - International Edition,2011,vol. 50,# 52,p. 12636 - 12638] Location in patent:supporting information; experimental part
879-05-0
32 suppliers
$153.00/50mL
1259-35-4
149 suppliers
$16.00/1g