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ChemicalBook CAS DataBase List TRI-N-BUTYLGERMANIUM CHLORIDE
2117-36-4

TRI-N-BUTYLGERMANIUM CHLORIDE synthesis

12synthesis methods
-

Yield:2117-36-4 95%

Reaction Conditions:

aluminium trichlorideother Radiation; a mixt. of GeCl4 and tetraalkylgermane in presence of AlCl3 as catalystin a Pyrex tube is irradiated with a light stream of argon for 3 min atatmospheric pressure (microwave irradiation: 300 W) (Ar); identification by (1)H-NMR, gas chromy.;

References:

Laurent, Régis;Laporterie, André;Dubac, Jacques;Berlan, Jacques [Organometallics,1994,vol. 13,# 6,p. 2493 - 2495]

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