Sulfamide synthesis
- Product Name:Sulfamide
- CAS Number:7803-58-9
- Molecular formula:H4N2O2S
- Molecular Weight:96.11
7791-25-5
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$15.00/0.5g
7664-41-7
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$15.00/100ml
7803-58-9
347 suppliers
$6.00/10g
Yield:7803-58-9 81%
Reaction Conditions:
in Petroleum etheraddn. of SO2Cl2 in dry petroleum ether to liquid NH3 (cooling: solid CO2 in CHCl3/CCl4); removal of cooling (removal of excess NH3); decanting of solvent; warming; - further information (to diminish vehemence of reaction) given;; extraction (soxhlet/CH3COOCH3); evapn.; drying (vac.); recrystn. from water; further information (extraction/increase of yield) given;;
References:
Degering, E. F.;Gross, G. C. [Industrial and Engineering Chemistry,1943,vol. 35,p. 751 - 753]
5329-14-6
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$13.50/100G
7803-58-9
347 suppliers
$6.00/10g
13598-81-7
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5329-14-6
497 suppliers
$13.50/100G
7803-58-9
347 suppliers
$6.00/10g
7791-25-5
265 suppliers
$15.00/0.5g
1074-82-4
482 suppliers
$5.00/25g
7803-58-9
347 suppliers
$6.00/10g
13598-81-7
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7803-63-6
156 suppliers
$14.00/100G
7803-58-9
347 suppliers
$6.00/10g