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    ChemicalBook CAS DataBase List Solifenacin Impurity 2
    1229227-22-8

    Solifenacin Impurity 2 synthesis

    1synthesis methods
    -

    Yield:-

    Steps:

    Multi-step reaction with 3 steps
    1: sodium tetrahydroborate; iodine / tetrahydrofuran / 16 h / Inert atmosphere; Reflux
    2: hydrogenchloride; borane-ammonia complex / aq. phosphate buffer / 37 °C / pH 7.8
    3: triethylamine / tetrahydrofuran / 2 h / 0 - 25 °C / Inert atmosphere

    References:

    Ghislieri, Diego;Green, Anthony P.;Pontini, Marta;Willies, Simon C.;Rowles, Ian;Frank, Annika;Grogan, Gideon;Turner, Nicholas J. [Journal of the American Chemical Society,2013,vol. 135,# 29,p. 10863 - 10869]

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