
(S)-1-Boc-3-hydroxymethyl-piperazine synthesis
- Product Name:(S)-1-Boc-3-hydroxymethyl-piperazine
- CAS Number:314741-40-7
- Molecular formula:C10H20N2O3
- Molecular Weight:216.28

147650-70-2
160 suppliers
$15.00/250mg

314741-40-7
175 suppliers
$9.00/100mg
Yield:-
Steps:
Multi-step reaction with 5 steps
1: 99 percent / sodium carbonate / H2O; tetrahydrofuran / 20 h / 23 °C
2: 39 g / potassium carbonate / dimethylformamide / 0 - 23 °C
3: 34.3 g / calcium chloride; sodium borohydride / ethanol / 0 - 20 °C
4: 27 g / ethyldiisopropylamine; methanesulfonic anhydride / 1,2-dichloro-ethane / 1 h / Heating
5: 21 g / lithium hydroxide monohydrate / H2O; ethanol / 1.5 h / Heating
References:
Gao, Hongwu;Renslo, Adam R. [Journal of Organic Chemistry,2007,vol. 72,# 22,p. 8591 - 8592]

314741-39-4
145 suppliers
$8.00/250mg

314741-40-7
175 suppliers
$9.00/100mg

848482-93-9
128 suppliers
$9.00/100mg

314741-40-7
175 suppliers
$9.00/100mg

24424-99-5
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$13.50/25G

126872-94-4
16 suppliers
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314741-40-7
175 suppliers
$9.00/100mg
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958635-18-2
26 suppliers
$64.00/100mg

314741-40-7
175 suppliers
$9.00/100mg