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ChemicalBook CAS DataBase List (S)-1-Boc-3-hydroxymethyl-piperazine
314741-40-7

(S)-1-Boc-3-hydroxymethyl-piperazine synthesis

9synthesis methods
(S) -1-BOC-3-hydroxymethylpiperazine can be used as an intermediate in organic synthesis, which can be synthesized from (S)-(4-benzylpiperazine-2-yl) methanol and methanol,with Palladium hydroxide on carbon.
147650-70-2 Synthesis
(S)-Piperazine-2-carboxylic acid

147650-70-2
160 suppliers
$15.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 99 percent / sodium carbonate / H2O; tetrahydrofuran / 20 h / 23 °C
2: 39 g / potassium carbonate / dimethylformamide / 0 - 23 °C
3: 34.3 g / calcium chloride; sodium borohydride / ethanol / 0 - 20 °C
4: 27 g / ethyldiisopropylamine; methanesulfonic anhydride / 1,2-dichloro-ethane / 1 h / Heating
5: 21 g / lithium hydroxide monohydrate / H2O; ethanol / 1.5 h / Heating

References:

Gao, Hongwu;Renslo, Adam R. [Journal of Organic Chemistry,2007,vol. 72,# 22,p. 8591 - 8592]

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