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ChemicalBook CAS DataBase List (R)-N-Boc-3-aminomethylpiperidine
140645-23-4

(R)-N-Boc-3-aminomethylpiperidine synthesis

7synthesis methods
37675-18-6 Synthesis
Ethyl (3S)-piperidine-3-carboxylate

37675-18-6
251 suppliers
$5.00/1g

-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 3 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C
3: dmap; triethylamine / dichloromethane / 3 h / 20 °C
4: sodium azide; sodium iodide / N,N-dimethyl-formamide / 4 h / 70 °C
5: hydrogen; 5%-palladium/activated carbon / methanol / 9 h / 20 °C

References:

KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY;HANDOK INC.;Jung, Hee Jung;Ha, Jae Du;Cho, Sung Yun;Kim, Hyoung Rae;Lee, Kwang Ho;Lee, Chong Ock;Choi, Sang Un;Park, Chi Hoon US2015/259350, 2015, A1

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