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ChemicalBook CAS DataBase List (R)-(-)-3-Pyrrolidinol hydrochloride
104706-47-0

(R)-(-)-3-Pyrrolidinol hydrochloride synthesis

4synthesis methods
(R)-3-Hydroxypyrrolidine hydrochloride is a pyrrole derivative, which can be used as a pharmaceutical intermediate. It can be synthesized by decarboxylation of trans-4-hydroxy-L-proline as a raw material.
109431-87-0 Synthesis
(R)-1-Boc-3-hydroxypyrrolidine

109431-87-0
360 suppliers
$5.00/1g

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Yield:104706-47-0 90%

Reaction Conditions:

with hydrogenchloride in 1,4-dioxane at 20; for 1 h;

Steps:

D108 Description D108(R)-Pyrrolidin-3-ol hydrochloride (Dl 08)

(R)-tert-Butyl 3-hydroxypyrrolidine-1 -carboxylate (250 mg, 1.34 mmol) was dissolved inHCI/dioxane (4 M, 5 mL) and stirred at rt for 1 h. The reaction mixture was concentrated to give the title compound (150 mg, yield 90%) as a white solid.1H NMR (300 MHz, DMSO-d6): 6 9.47 (br s, I H), 9.24 (br 5, 1 H), 4.38 (s, 1 H), 3.57-2.96 (m, 4H), 1.95-1.79 (m, 2H).

References:

WO2017/12576,2017,A1 Location in patent:Page/Page column 117

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