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329976-79-6

POTASSIUM OCTYLTRIFLUOROBORATE synthesis

6synthesis methods
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Yield:329976-79-6 71%

Reaction Conditions:

Stage #1: Trimethyl borate;octylmagnesium bromide in tetrahydrofuran at -78 - 0; for 1.83333 h;
Stage #2: with potassium hydrogen difluoride;water in tetrahydrofuran at 0 - 20; for 1.16667 h;

References:

Reichle, Markus A.;Breit, Bernhard [Angewandte Chemie - International Edition,2012,vol. 51,# 23,p. 5730 - 5734] Location in patent:supporting information; experimental part

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