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ChemicalBook CAS DataBase List N-NONACOSANE
630-03-5

N-NONACOSANE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: benzophenone; N-hydroxyphthalimide / 62 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: benzophenone; N-hydroxyphthalimide / 48 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation
4.1: ethanol / 24 h / 20 °C
5.1: sodium tetrahydroborate / dichloromethane; methanol / 0 - 20 °C
5.2: 24 h / 20 °C

References:

Guin, Joyram;Paul, Subhasis [Chemistry - A European Journal,2021,vol. 27,# 13,p. 4412 - 4419]

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