ChemicalBook CAS DataBase List N,N-Dimethylethylamine

N,N-Dimethylethylamine synthesis

11synthesis methods

Product Name:N,N-Dimethylethylamine
CAS Number:598-56-1
Molecular formula:C4H11N
Molecular Weight:73.14

127-19-5 Synthesis

127-19-5
825 suppliers
$5.00/25g

598-56-1
165 suppliers
$22.57/100 mL

624-78-2 Synthesis

624-78-2
255 suppliers
$16.00/1g

616-39-7
120 suppliers
$5.00/1g

Yield:598-56-1 96.1 %Chromat. ，624-78-2 2.8 %Chromat. ，616-39-7 0.8 %Chromat.

Reaction Conditions:

with hydrogen;dimethyl amine;Cu-Cr catalyst Cu₀₂₀₃ Engelhard at 250; under 7500.75 Torr;Product distribution / selectivity;Gas phase;

Steps:

3
Example 3: In a fixed bed reactor containing 5 g of catalyst (Cu0203 Engelhard) a mixture of N,N-dimethylacetamide, DMA and H₂ is introduced. The mixture with a molar composition of amide/auxiliary amine/H₂ of 1/3/30 is preheated and introduced continuously at the catalyst bed at a rate of 2 g amide/h. The reactor is heated at 25CO and operated at 10 bars. At the outlet, the product containing the desired amine is analysed with GC on-line. The product composition (area%) is displayed in table 3.

References:

TAMINCO WO2006/136204, 2006, A1 Location in patent:Page/Page column 13

18871-66-4 Synthesis